ammonia in acetonitrile t-BuSnMe3 in CH3CN added to Fe(phen)3(ClO4)3 in CH3CN at 22°C under Ar and soln. stirred for 2 h, drop water added, Fe(II) complex filtered, filtrate dried with MgSO4 and treated with anhyd. aq. NH3, Sn product treated with HCl and sublimed;
参考文献
Journal of the American Chemical Society, , vol. 104, # 5 p. 1319 - 1330
Rollick; Kochi
Journal of the American Chemical Society, 1982 , vol. 104, # 5 p. 1319 - 1330
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反应条件
ammonia in acetonitrile t-BuSnMe3 in CH3CN added to Fe(phen)3(ClO4)3 in CH3CN at 22°C under Ar and soln. stirred for 2 h, drop water added, Fe(II) complex filtered, filtrate dried with MgSO4 and treated with anhyd. aq. NH3, Sn product treated with HCl and sublimed;
参考文献
Journal of the American Chemical Society, , vol. 104, # 5 p. 1319 - 1330
