2-氰基-3-乙氧基巴豆酸乙酯合成路线 （共 14 条）
反应条件
acetic anhydride 3 h; Reflux;
参考文献
Bamoharram, Fatemeh F.; Roshani, Minaa; Heravi, Majid M.; Mahdavi, Masoumeh; Javid, Alia; Emampour, Jalal Sh.
Chinese Journal of Chemistry, 2010 , vol. 28, # 6 p. 974 - 976
参考文献
Popp,F.D.; Catala,A.
Journal of Organic Chemistry, 1961 , vol. 26, p. 2738 - 2740
参考文献
Haller
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1900 , vol. 130, p. 1224
反应条件
hydrazine hydrate in acetic acid 0.5 h; Heating;
参考文献
Huppatz, John L.
Australian Journal of Chemistry, 1985 , vol. 38, # 1 p. 221 - 230
反应条件
1: 57 percent / EtONa / ethanol / 7 h / Heating 2: 47 percent / ethanol / 1 h / Heating View Scheme
参考文献
McFadden, Helen G.; Huppatz, John L.; Halladay, Peter K.
Australian Journal of Chemistry, 1993 , vol. 46, # 6 p. 873 - 886
反应条件
potassium acetate in ethanol 2 h; Heating;
参考文献
Saito, Koji; Kambe, Satoshi; Sakurai, Akio; Midorikawa, Hiroshi
Synthesis, 1982 , # 12 p. 1056 - 1059
反应条件
hydroxylamine hydrochloride; sodium methylate in ethanol
参考文献
Bamoharram, Fatemeh F.; Roshani, Minaa; Heravi, Majid M.; Mahdavi, Masoumeh; Javid, Alia; Emampour, Jalal Sh.
Chinese Journal of Chemistry, 2010 , vol. 28, # 6 p. 974 - 976
反应条件
silica gel in N,N-dimethyl acetamide 0.15 h; microwave irradiation;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 181, # 3 p. 591 - 599
反应条件
1.1: 2 h / 70 °C
2.1: acetic acid / Reflux
2.2: pH ~ 9 - 10
View Scheme
参考文献
DECIPHERA PHARMACEUTICALS, LLC; FLYNN, Daniel L.; KAUFMAN, Michael D.
Patent: WO2013/78295 A2, 2013 ;
反应条件
in ethanol
4 h; Heating;
参考文献
Khan, Misbahul A.; Jorge, Tereza C. M.
Monatshefte fuer Chemie, 1983 , vol. 114, p. 333 - 338
