O-丙-2-基甲硫基甲烷硫酸酯合成路线 （共 9 条）
反应条件
1: carbon disulfide; isopropyl alcohol in dimethyl sulfoxide T=20°C; 0.333333 h; 2: With N-benzyl-trimethylammonium hydroxide in dimethyl sulfoxide T=20°C; 1 h; 3: methyl iodide in dimethyl sulfoxide T=20°C; 2.5 h;
参考文献
Chaturvedi, Devdutt; Ray, Suprabhat
Monatshefte fur Chemie, 2006 , vol. 137, # 9 p. 1219 - 1223
反应条件
sodium hydride in tetrahydrofuran; paraffin 1 h; Ambient temperature;
参考文献
Sun, Wei Yan; Hu, Ji Qing; Shi, Yong Ping
Synlett, 1997 , vol. 1997, # 11 p. 1279 - 1280
参考文献
Wertheim
Journal of the American Chemical Society, 1931 , vol. 53, p. 4042
参考文献
Mott, Andrew W.; Barany, George
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2615 - 2621
反应条件
4-(1-piperidino)pyridine T=110°C; Rearrangement; 4 h;
参考文献
Organic Preparations and Procedures International, , vol. 24, # 2 p. 200 - 204
反应条件
sulfuryl dichloride in chloroform-d1 T=25°C; 0.166667 h; Yield given. Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 11 p. 2615 - 2621
反应条件
T=226.9 - 276.9°C; pyrolysis, ΔH(excit.), ΔS(excit.), k629/s; KineticsMechanismThermodynamic data;
参考文献
Al-Awadi, Nouria; Bigley, David B.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1982 , p. 773 - 776
反应条件
sulfuryl dichloride
1.) <2H>chloroform, 25 deg C, 10 min, 2.) chloroform, 25 deg C, 5 min; Yield given. Multistep reaction. Title compound not separated from byproducts;
参考文献
Mott, Andrew W.; Barany, George
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2615 - 2621
反应条件
sulfuryl dichloride in chloroform-d1
T=25°C; 0.166667 h; Yield given. Title compound not separated from byproducts;
参考文献
Mott, Andrew W.; Barany, George
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2615 - 2621
