(2-([2-(羟基甲基)苯基]二磺酰基)苯基)甲醇合成路线 (共 9 条)
反应条件
aluminum oxide in neat (no solvent) 0.333333 h; Milling; chemoselective reaction;
参考文献
Chatterjee, Tanmay; Ranu, Brindaban C.
RSC Advances, 2013 , vol. 3, # 27 p. 10680 - 10686
反应条件
borane-THF; boron trifluoride diethyl etherate in tetrahydrofuran T=20°C; 18 h;
参考文献
Chen; Iakovleva; Kesten; Magano; Rodriguez; Sexton; Zhang; Lee
Organic Preparations and Procedures International, 2002 , vol. 34, # 6 p. 665 - 670
反应条件
in toluene 96 h; Heating;
参考文献
Davis, Franklin A.; Jenkins, Linda A.; Billmers, Robert L.
Journal of Organic Chemistry, 1986 , vol. 51, # 7 p. 1033 - 1040
反应条件
in toluene 72 h; Heating;
参考文献
Davis, Franklin A.; Jenkins, Linda A.; Billmers, Robert L.
Journal of Organic Chemistry, 1986 , vol. 51, # 7 p. 1033 - 1040
反应条件
lithium aluminium tetrahydride; diethyl ether anschliessende Oxidation mit Jod;
参考文献
Costanza et al.
Journal of Polymer Science, 1955 , vol. 17, p. 319,327
反应条件
1: LiAlH4 2: aq. I2 View Scheme
参考文献
Grice,R.; Owen,L.N.
Journal of the Chemical Society, 1963 , p. 1947 - 1954
反应条件
dann beim Eintragen in siedendes Wasser oder besser beim Ruehren mit Wasser bei Raumtemperatur;
参考文献
Reissert; Craemer
Chemische Berichte, 1928 , vol. 61, p. 2559
参考文献
Reissert; Craemer
Chemische Berichte, 1928 , vol. 61, p. 2559
反应条件
1: 16 percent / PCC
2: 80 percent / Ph3P / dimethylformamide; H2O; methanol / 1.) room temp., 30 min; 2.) ice-water bath, 30 min
View Scheme
参考文献
THE BOARD OF TRUSTEES OF THE UNIVERSITY OF ILLINOIS
Patent: WO2008/134474 A2, 2008 ;
Location in patent: Page/Page column 77 ;