3,3'-亚氨基二丙酸二乙酯合成路线 （共 23 条）
反应条件
ethanol; sodium ethanolate
参考文献
Ruzicka; Fornasir
Helvetica Chimica Acta, 1920 , vol. 3, p. 812
反应条件
das Hydrochlorid liefert;
参考文献
Ruzicka; Fornasir
Helvetica Chimica Acta, 1920 , vol. 3, p. 812
反应条件
1: 60 percent / LiAlH4 / diethyl ether / 5 h / 25 °C 2: 60 percent / SO2Cl2 / CHCl3 / 3 h / Heating View Scheme
参考文献
Hahn, Ekkehardt F.; Rupprecht, Stefan
Chemische Berichte, 1991 , vol. 124, # 3 p. 481 - 486
反应条件
1: benzene 2: sodium; ethanol; benzene 3: Raney nickel; ethanol / 120 °C / 128714 Torr / Hydrogenation 4: HCl / 180 - 200 °C View Scheme
参考文献
McElvain; Stork
Journal of the American Chemical Society, 1946 , vol. 68, p. 1049,1052
反应条件
1: 1.) HO-, 2.) H3O+ 2: BH3*S(CH3)2 3: pyridine / acetonitrile 4: KH / dimethylformamide 5: HBr 6: KOH / methanol View Scheme
参考文献
Erhardt,J.M.; Grover,E.R.; Wuest,J.D.
Journal of the American Chemical Society, 1980 , vol. 102, p. 6365
反应条件
sodium hydroxide 1.) 1h, 2.) 1h, reflux;
参考文献
Beddoes, Roy L.; Edwards, W. D.; Joule, J. A.; Mills, O. S.; Street, J. D.
Tetrahedron, 1987 , vol. 43, # 8 p. 1903 - 1920
参考文献
Kuettel; McElvain
Journal of the American Chemical Society, 1931 , vol. 53, p. 2692,2696
反应条件
lithium aluminium tetrahydride in diethyl ether T=25°C; 5 h;
参考文献
Hahn, Ekkehardt F.; Rupprecht, Stefan
Chemische Berichte, 1991 , vol. 124, # 3 p. 481 - 486
反应条件
1: 1.) HO-, 2.) H3O+ 2: BH3*S(CH3)2 3: pyridine / acetonitrile 4: KH / dimethylformamide 5: HBr View Scheme
参考文献
Erhardt,J.M.; Grover,E.R.; Wuest,J.D.
Journal of the American Chemical Society, 1980 , vol. 102, p. 6365
参考文献
Edwards,D. et al.
Journal of Pharmacy and Pharmacology, 1964 , vol. 16, p. 618 - 626
