2'-羟基-3-苯基苯丙酮合成路线 (共 38 条)
反应条件
10 Pd/C; 4,4'-diphenylsulfide; hydrogen in methanol T=20°C; 24 h; chemoselective reaction;
参考文献
Mori, Akinori; Mizusaki, Tomoteru; Kawase, Masami; Maegawa, Tomohiro; Monguchi, Yasunari; Takao, Shinobu; Takagi, Yukio; Sajikia, Hironao
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 3 p. 406 - 410
反应条件
ammonium formate; palladium on activated charcoal in tetrahydrofuran; methanol T=20°C; 0.55 h;
参考文献
Ahmed, Naseem; Van Lier, Johan E.
Journal of Chemical Research, 2006 , # 9 p. 584 - 585
反应条件
2,9-dimethyl-1,10-phenanthroline; palladium diacetate; silver carbonate in acetonitrile T=60°C; 24 h; regioselective reaction;
参考文献
Vellakkaran, Mari; Andappan, Murugaiah M. S.; Kommu, Nagaiah
European Journal of Organic Chemistry, 2012 , # 25 p. 4694 - 4698
反应条件
potassium hydroxide; tris(triphenylphosphine)ruthenium(II) chloride in 1,4-dioxane T=80°C; 40 h;
参考文献
Cho, Chan Sik; Shim, Sang Chul
Journal of Organometallic Chemistry, 2006 , vol. 691, # 20 p. 4329 - 4332
反应条件
lithium tert-butylate in toluene T=110°C; 12 h; Inert atmosphere;
参考文献
Liang, Yu-Feng; Zhou, Xin-Feng; Tang, Shi-Ya; Huang, Yao-Bing; Feng, Yi-Si; Xu, Hua-Jian
RSC Advances, 2013 , vol. 3, # 21 p. 7739 - 7742
反应条件
potassium phosphate; [RhCl(η2:η2-cycloocta-1,5-diene)]2; (Ra,R,R)-SIPHOS-PE in 1,2-dichloro-ethane T=70°C; 36 h; Inert atmosphere; Overall yield = 98 percent;
参考文献
Von Delius, Max; Le, Christine M.; Dong, Vy M.
Journal of the American Chemical Society, 2012 , vol. 134, # 36 p. 15022 - 15032
反应条件
hydrogen; boric acid; nickel in methanol; water
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 42, # 5 p. 303 - 308
反应条件
methanesulfonic acid; trifluoromethanesulfonic anhydride T=65°C; Fries rearrangement; Inert atmosphere; regioselective reaction;
参考文献
Jeon, Ingyu; Mangion, Ian K.
Synlett, 2012 , vol. 23, # 13 p. 1927 - 1930
反应条件
lithium tert-butylate in N,N-dimethyl-formamide T=60°C; 12 h;
参考文献
European Journal of Organic Chemistry, , # 11 p. 2080 - 2083
反应条件
Rhodococcus sp. DSM 364 in acetone T=28°C; 168 h; Microbiological reaction;
参考文献
Journal of Molecular Catalysis B: Enzymatic, , vol. 97, p. 283 - 288