2,4-二氯-N,N-二甲基苯胺合成路线 (共 12 条)
反应条件
iodobenzene; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; lithium chloride in tetrahydrofuran T=20°C; 24 h;
参考文献
Li, Ting-Ting; Xu, Cui; Xiang, Chang-Bin; Yan, Jie
Chinese Chemical Letters, 2013 , vol. 24, # 6 p. 535 - 538
反应条件
hydrogenchloride; sodium chlorate
参考文献
Cassella and Co.
Patent: DE453427 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 16, p. 366
反应条件
Basolite® A100 T=170°C; 8 h;
参考文献
Dhakshinamoorthy, Amarajothi; Alvaro, Mercedes; Garcia, Hermenegildo
Applied Catalysis A: General, 2010 , vol. 378, # 1 p. 19 - 25
参考文献
Borkowski; Wagner
Journal of Organic Chemistry, 1952 , vol. 17, p. 1128,1132
反应条件
N-chlorotriethylammonium chloride in trifluoroacetic acid Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Smith, John R. Lindsay; McKeer, Linda C.; Taylor, Jonathan M.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 385 - 392
参考文献
Schmidt; Schumacher
Chemische Berichte, 1921 , vol. 54, p. 1417
反应条件
trichloroisocyanuric acid; sulfuric acid 20 h; Ambient temperature; Further byproducts given;
参考文献
Rosevear, Judi; Wilshire, John F. K.
Australian Journal of Chemistry, 1980 , vol. 33, # 4 p. 843 - 852
反应条件
trichloroisocyanuric acid; sulfuric acid 20 h; Ambient temperaturevar. subst. N,N-dimethylanilines and Fischer base; dichloroisocyanuric acid as reagent; Product distribution;
参考文献
Rosevear, Judi; Wilshire, John F. K.
Australian Journal of Chemistry, 1980 , vol. 33, # 4 p. 843 - 852
参考文献
Krell
Chemische Berichte, 1872 , vol. 5, p. 878
Full Text Show Details
Fries; Glahn
Justus Liebigs Annalen der Chemie, 1906 , vol. 346, p. 147 Anm.
参考文献
Danilow; Kosmina
Zhurnal Obshchei Khimii, 1949 , vol. 19, p. 309,312
J. Gen. Chem. USSR (Engl. Transl.), 1949 , vol. 19, p. 269