2,3,5,6-四氟-4-硝基吡啶合成路线 (共 5 条)
反应条件
ammonium chloride; zinc in ethanol; water T=50 - 60°C;
参考文献
Miller, A.O.; Furin, G. G.
Journal of Fluorine Chemistry, 1987 , vol. 36, p. 247 - 272
反应条件
in neat (no solvent) 600 °C (1.5 h);;
参考文献
Gmelin Handbook: F: PerFHalOrg.5, 4, page 115 - 148
反应条件
ammonium chloride; zinc in ethanol; water T=50 - 60°C;
参考文献
Miller, A.O.; Furin, G. G.
Journal of Fluorine Chemistry, 1987 , vol. 36, p. 247 - 272
反应条件
1: zinc powder, NH4Cl / H2O; ethanol / 50 - 60 °C 2: 10 h / 120 - 125 °C View Scheme
参考文献
Miller, A.O.; Furin, G. G.
Journal of Fluorine Chemistry, 1987 , vol. 36, p. 247 - 272
反应条件
in diethyl ether
0 °C, 4 h, dry ether;; chromatography;;
参考文献
Gmelin Handbook: F: PerFHalOrg.5, 4.1.1.3, page 180 - 219