N-[(4-甲氧基苯基)甲基]乙酰胺合成路线 (共 48 条)
反应条件
bromine in dichloromethane; water T=20°C; Oxidation; bromination; 5 h; Irradiation; Product distribution; Further Variations:Solvents;
参考文献
Journal of Organic Chemistry, , vol. 65, # 12 p. 3880 - 3881
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=70°C;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 18, # 8 p. 2714 - 2718
参考文献
Sekiya,M. et al.
Chemical and Pharmaceutical Bulletin, 1961 , vol. 9, # 12 p. 945 - 948
反应条件
sulfuric acid in water T=60 - 92°C; ΔH(excit.), ΔS(excit.); KineticsMechanismThermodynamic data;
参考文献
Druet, Linda M.; Yates, Keith
Canadian Journal of Chemistry, 1984 , vol. 62, p. 2401 - 2414
反应条件
potassium fluoride; (NH4)2S2O8; CuSO4‵5H2O; silver nitrate in water
T=20°C; 6 h; Inert atmosphere;
参考文献
Itoh, Izuho; Matsusaki, Yoko; Fujiya, Akitoshi; Tada, Norihiro; Miura, Tsuyoshi; Itoh, Akichika
Tetrahedron Letters, 2014 , vol. 55, # 20 p. 3146 - 3148
反应条件
2-hydroxy-1,3-isoindolinedione; oxygen; anhydrous cobalt diacetate; metachloroperbenzoic acid in acetonitrile
T=20°C; 2 h; Title compound not separated from byproducts.;
参考文献
Minisci, Francesco; Punta, Carlo; Recupero, Francesco; Fontana, Francesca; Franco Pedulli, Gian
Journal of Organic Chemistry, 2002 , vol. 67, # 8 p. 2671 - 2676
反应条件
2-hydroxy-1,3-isoindolinedione; oxygen; anhydrous cobalt diacetate in acetic acid
T=100°C; 1 h; Title compound not separated from byproducts.;
参考文献
Minisci, Francesco; Punta, Carlo; Recupero, Francesco; Fontana, Francesca; Franco Pedulli, Gian
Journal of Organic Chemistry, 2002 , vol. 67, # 8 p. 2671 - 2676
反应条件
1: nitric acid
2: tin; hydrochloric acid
View Scheme
参考文献
Goldschmidt; Polonowska
Chemische Berichte, 1887 , vol. 20, p. 2407