3-烯丙基戊烷-2,4-二酮合成路线 (共 34 条)
反应条件
copper; Cu(II) perchlorate in diethyl ether 1 h; Ambient temperature;
参考文献
Baruah, Jubaraj B.; Samuelson, Ashoka G.
Journal of Organometallic Chemistry, 1989 , vol. 361, p. C57 - C60
反应条件
triethylamine; triphenylphosphine; polystyrene; palladium in tetrahydrofuran T=65°C; 12 h;
参考文献
Bergbreiter, David E.; Chen, Bushi
Journal of the Chemical Society, Chemical Communications, 1983 , # 21 p. 1238 - 1239
反应条件
sodium ethanolate in diethyl ether Condensation; 2 h; Heating;
参考文献
Voloshanovskii; Manaeva; Shevchenko; Mamontov
Russian Journal of Applied Chemistry, 2000 , vol. 73, # 2 p. 296 - 300
反应条件
sodium hydroxide in water 40 h; Ambient temperaturepH 8.0; Title compound not separated from byproducts;
参考文献
King; Rathore; Lam; Guo; Klassen
Journal of the American Chemical Society, 1992 , vol. 114, # 8 p. 3028 - 3033
反应条件
bis-diphenylphosphinoethane; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran 2 h; Ambient temperature;
参考文献
Suzuki, Osamu; Hashiguchi, Yoshiharu; Inoue, Seiichi; Sato, Kikumasa
Chemistry Letters, 1988 , p. 291 - 294
反应条件
1,2-bis-(diphenylphosphino)ethane; bis(dibenzylideneacetone)-palladium(0) in N,N-dimethyl-formamide 1 h; Ambient temperature;
参考文献
Suzuki, Osamu; Inoue, Seiichi; Sato, Kikumasa
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 1 p. 239 - 243
反应条件
copper; Cu(II) perchlorate in tetrahydrofuran 8 h; Heating;
参考文献
Baruah, Jubaraj B.; Samuelson, Ashoka G.
Journal of Organometallic Chemistry, 1989 , vol. 361, p. C57 - C60
反应条件
ceric tetrabutylammonium nitrate in acetonitrile 4 h;
参考文献
Zhang, Yang; Raines, Andrew J.; Flowers II, Robert A.
Organic Letters, 2003 , vol. 5, # 13 p. 2363 - 2365
反应条件
1: 1.64 g / Amberlyst H-15; molecular sieves 4 Angstroem / pentane / 48 h 2: 62 percent / CTAN / acetonitrile / 4 h / 20 °C View Scheme
参考文献
Zhang, Yang; Raines, Andrew J.; Flowers II, Robert A.
Journal of Organic Chemistry, 2004 , vol. 69, # 19 p. 6267 - 6272
反应条件
sodium hydroxide anschliessend Erwaermen mit Allylbromid;
参考文献
Davis; Hurd
Journal of the American Chemical Society, 1955 , vol. 77, p. 3284,3287