3-烯丙基戊烷-2,4-二酮合成路线 (共 34 条)
反应条件
tetrabutylammomium bromide; potassium carbonate; palladium dichloride in water Tsuji-Trost reaction; 9 h; Heating;
参考文献
Ranu, Brindaban C.; Chattopadhyay, Kalicharan; Adak, Laksmikanta
Organic Letters, 2007 , vol. 9, # 22 p. 4595 - 4598
反应条件
[RhCl(η2:η2-cycloocta-1,5-diene)]2; PTA in water; ethyl acetate T=20°C; 3.5 h; Inert atmosphere;
参考文献
Komine, Nobuyuki; Ishiguro, Kohtaro; Kanai, Sachiyo; Hirano, Masafumi; Komiya, Sanshiro
Journal of Organometallic Chemistry, 2011 , vol. 696, # 10 p. 1927 - 1930
反应条件
copper; Cu(II) perchlorate; ethyl acetate 12 h; Heating;
参考文献
Baruah, Jubaraj B.; Samuelson, Ashoka G.
Journal of Organometallic Chemistry, 1989 , vol. 361, p. C57 - C60
反应条件
P(MeNCH2CH2)3N in hexane; acetonitrile T=25°C; 0.5 h;
参考文献
Arumugam, Subramaniam; McLeod, Dale; Verkade, John G.
Journal of Organic Chemistry, 1998 , vol. 63, # 11 p. 3677 - 3679
反应条件
(pentamethylcyclopentadienyl)Ru(1,5-cyclooctadiene)Cl in 1,2-dichloro-ethane T=90°C; 6 h;
参考文献
Yamamoto, Yoshihiko; Nakagai, Yu-Ichiro; Itoh, Kenji
Chemistry - A European Journal, 2004 , vol. 10, # 1 p. 231 - 236
反应条件
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; (R,R)-anthracenyl Trost ligand in 1,4-dioxane T=20°C; 0.25 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Trost, Barry M.; Xu, Jiayi; Schmidt, Thomas
Journal of the American Chemical Society, 2009 , vol. 131, # 51 p. 18343 - 18357
反应条件
tetrakis(triphenylphosphine) palladium(0); 18-crown-6 ether; carbon dioxide; potassium carbonate T=75°C; Tsuji-Trost Allylation; P=57003.8 Torr; 18 h; Supercritical conditionsAutoclave;
参考文献
Laurenti; Feuerstein; Pepe; Doucet; Santelli
Journal of Organic Chemistry, 2001 , vol. 66, # 5 p. 1633 - 1637
反应条件
CTAN in acetonitrile T=20°C; 4 h;
参考文献
Zhang, Yang; Raines, Andrew J.; Flowers II, Robert A.
Journal of Organic Chemistry, 2004 , vol. 69, # 19 p. 6267 - 6272
反应条件
1: in acetonitrile T=20°C; 2: With triethylamine in hexane; ethyl acetate T=20°C; 0.5 h;
参考文献
Zhang, Yang; Raines, Andrew J.; Flowers II, Robert A.
Journal of Organic Chemistry, 2004 , vol. 69, # 19 p. 6267 - 6272
反应条件
sulfuric acid; iodine in dimethyl sulfoxide T=60°C; 0.5 h; Acidic conditions;
参考文献
Nawghare, Beena R.; Lokhande, Pradeep D.
Synthetic Communications, 2013 , vol. 43, # 14 p. 1955 - 1963