3-二甲基氨基-1-苯丙烷-1-酮合成路线 （共 69 条）
反应条件
T=20°C; 13 h; Ionic liquid;
参考文献
Rashinkar, Gajanan; Pore, Santoshkumar; Salunkhe, Rajeshree
Phosphorus, Sulfur and Silicon and the Related Elements, 2009 , vol. 184, # 7 p. 1750 - 1758
反应条件
5-(2-hydroxyethyl)-4-methyl-3-(phenylmethyl)thiazolium chloride; triethylamine in N,N-dimethyl-formamide
参考文献
Stetter,H. et al.
Chemische Berichte, 1977 , vol. 110, p. 1971 - 1977
参考文献
Jacob; Madinaveitia
Journal of the Chemical Society, 1937 , p. 1929
反应条件
in acetonitrile
4 h; Heating;
参考文献
Bravo, Pierfrancesco; Ticozzi, Calimero; Cavicchio, Giancarlo
Synthesis, 1985 , # 9 p. 894 - 896
反应条件
3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide; triethylamine in N,N-dimethyl-formamide
T=85°C;
参考文献
Jones, R. Alan; Karatza, Marielena; Voro, Tevita N.; Civcir, Pervin U.; Franck, Annete; Ozturk, Orhan; Seaman, John P.; Whitmore, Alexander P.; Williamson, David J.
Tetrahedron, 1996 , vol. 52, # 26 p. 8707 - 8724
反应条件
in tetrahydrofuran
1 h; Ambient temperature;
参考文献
Aoyama, Hiromu; Sugiyama, Jun-ichi; Yoshida, Masamichi; Hatori, Hiroaki; Hosomi, Akira
Journal of Organic Chemistry, 1992 , vol. 57, # 11 p. 3037 - 3041
反应条件
1: With (dppf)RuCl2(enethylenediamine); potassium tert-butylate; hydrogen in isopropyl alcohol
T=70°C; P=7757.43 Torr; Inert atmosphereSchlenk technique;
2: With hydrogenchloride in water; acetone
Inert atmosphereSchlenk technique;
参考文献
De Koning, Pieter D.; Jackson, Mark; Lennon, Ian C.
Organic Process Research and Development, 2006 , vol. 10, # 5 p. 1054 - 1058
反应条件
T=20°C; 14 h; Ionic liquid;
参考文献
Rashinkar, Gajanan; Pore, Santoshkumar; Salunkhe, Rajeshree
Phosphorus, Sulfur and Silicon and the Related Elements, 2009 , vol. 184, # 7 p. 1750 - 1758
参考文献
Mannich; Heilner
Chemische Berichte, 1922 , vol. 55, p. 362
