5-[(Z)-[(5E)-5-[[5-[(Z)-(3,4-二乙基-5-氧代吡咯-2-亚基)甲基]-3,4-二乙基-1H-吡咯-2-基]亚甲基]-3,4-二乙基吡咯-2-亚基]甲基]-3,4-二乙基吡咯-2-酮合成路线 （共 9 条）
反应条件
oxygen in acetic acid T=80 - 90°C; 22 h;
参考文献
Bonnett, Raymond; Buckley, Dennis G.; Hamzetash, Dariush
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 322 - 325
反应条件
hydrogenchloride in diethyl ether 25 h; Ambient temperature;
参考文献
Bonnett, Raymond; Buckley, Dennis G.; Hamzetash, Dariush
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 322 - 325
反应条件
1: 1.) POCl3, 2.) NaHCO3, ice / 1.) ice cooling, 15 min, 40-50 deg C, overnight, 2.) pH 8-9, 90 deg C, 10-15 min 2: 61 percent / aq. NaOH / ethanol / 20 h / Heating 3: 90 percent / anhyd. HCl / diethyl ether / 25 h / Ambient temperature View Scheme
参考文献
Bonnett, Raymond; Buckley, Dennis G.; Hamzetash, Dariush
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 322 - 325
反应条件
1: 26 percent / aq. NaOH / ethanol / 22 h / Heating 2: 25 percent / oxygen / acetic acid / 22 h / 80 - 90 °C View Scheme
参考文献
Bonnett, Raymond; Buckley, Dennis G.; Hamzetash, Dariush
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 322 - 325
反应条件
1: 61 percent / aq. NaOH / ethanol / 20 h / Heating 2: 90 percent / anhyd. HCl / diethyl ether / 25 h / Ambient temperature View Scheme
参考文献
Bonnett, Raymond; Buckley, Dennis G.; Hamzetash, Dariush
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 322 - 325
反应条件
in tetrahydrofuran; methanol 4.5 h; Irradiation;
参考文献
Bonnett, Raymond; Chaney, Brian D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1063 - 1068
反应条件
in pyridine 48 h; Ambient temperature; Further byproducts given;
参考文献
Saito, Setsuo; Itano, Harvey A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1183 - 1188
反应条件
in methanol; benzene 72 h; Irradiation;
参考文献
Bonnett, Raymond; Chaney, Brian D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1063 - 1068
反应条件
in tetrahydrofuran; methanol 70 h; Irradiationvarious time of irradiation, and solvent mixture; Product distribution;
参考文献
Bonnett, Raymond; Chaney, Brian D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1063 - 1068
