(S)-(-)-2-甲基丁胺合成路线 （共 17 条）
反应条件
hydrazine hydrate in ethanol 10 h; Heating;
参考文献
Wang, Chun-Jiang; Sun, Xianfeng; Zhang, Xumu
Angewandte Chemie - International Edition, 2005 , vol. 44, # 31 p. 4933 - 4935
反应条件
1: 98.5 percent / hydrogen / RuCl2[(S)-C3-TunePhos](DMF)m / methanol / 16 h / 50 °C / 76000 Torr 2: 65 percent / hydrazine monohydrate / ethanol / 10 h / Heating View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 44, # 31 p. 4933 - 4935
反应条件
1: triphenylphosphine; diethyl azodicarboxylate / 0 - 20 °C 2: 98.5 percent / hydrogen / RuCl2[(S)-C3-TunePhos](DMF)m / methanol / 16 h / 50 °C / 76000 Torr 3: 65 percent / hydrazine monohydrate / ethanol / 10 h / Heating View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 44, # 31 p. 4933 - 4935
反应条件
methanol; platinum(IV) oxide P=2206.5 Torr; Hydrogenation;
参考文献
Journal of Biological Chemistry, , vol. 115, p. 426
反应条件
1: pyridine 2: NaN3 / dimethylformamide 3: LiAlH4 / diethyl ether View Scheme
参考文献
Helvetica Chimica Acta, , vol. 86, # 2 p. 274 - 279
反应条件
sodium tetrahydroborate; nickel dichloride in N,N-dimethyl-formamide T=20°C;
参考文献
Synlett, , # 4 p. 542 - 546
反应条件
1: NaN3 / dimethylformamide 2: LiAlH4 / diethyl ether View Scheme
参考文献
Helvetica Chimica Acta, , vol. 86, # 2 p. 274 - 279
参考文献
Anteunis, M. J. O.; Callens, R.; Witte, M. De; Reyniers, M. F.; Spiessens, L.
Bulletin des Societes Chimiques Belges, 1987 , vol. 96, # 7 p. 545 - 554
反应条件
1: 50 percent / various solvent(s) / 24 h / 85 °C 2: 90 percent / 1 N HCl / various solvent(s) 3: 69 percent / KOH View Scheme
参考文献
Bulletin des Societes Chimiques Belges, , vol. 96, # 7 p. 545 - 554
反应条件
1: 90 percent / 1 N HCl / various solvent(s) 2: 69 percent / KOH View Scheme
参考文献
Bulletin des Societes Chimiques Belges, , vol. 96, # 7 p. 545 - 554
