2-氰-3,3-二(甲硫基)丙烯酸甲酯合成路线 （共 33 条）
反应条件
hydrogenchloride; triethylamine in ethanol Heating;
参考文献
Kohra, Shinya; Tominaga, Yoshinori; Hosomi, Akira
Journal of Heterocyclic Chemistry, 1988 , vol. 25, p. 959 - 968
反应条件
1: 89 percent / 1.) triethylamine; 2.) 10percent HCl / ethanol / 5 h / Heating 2: 86 percent / POCl3, N,N-dimethylaniline / 2 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 25, p. 959 - 968
反应条件
1: 1.7 percent / NaH / dimethylformamide / 4 h / Ambient temperature 2: phosphorus oxychloride View Scheme
参考文献
Kohra, Shinya; Tominaga, Yoshinori; Hosomi, Akira
Journal of Heterocyclic Chemistry, 1988 , vol. 25, p. 959 - 968
反应条件
hydrogenchloride; sodium hydride in N,N-dimethyl acetamide; benzene
20 h; Ambient temperature;
参考文献
Kohra, Shinya; Tominaga, Yoshinori; Hosomi, Akira
Journal of Heterocyclic Chemistry, 1988 , vol. 25, p. 959 - 968
反应条件
potassium hydroxide in N,N-dimethyl-formamide
6 h; Ambient temperature;
参考文献
Mizuyama, Naoko; Murakami, Yuka; Kohra, Shinya; Ueda, Kazuo; Hiraoka, Kyoko; Nagaoka, Junko; Takahashi, Kojiro; Shigemitsu, Yasuhiro; Tominaga, Yoshinori
Journal of Heterocyclic Chemistry, 2007 , vol. 44, # 1 p. 115 - 132
反应条件
sodium hydroxide in dimethyl sulfoxide
T=20°C; 3 h;
参考文献
Mizuyama, Naoko; Murakami, Yuka; Kohra, Shinya; Ueda, Kazuo; Hiraoka, Kyoko; Nagaoka, Junko; Takahashi, Kojiro; Shigemitsu, Yasuhiro; Tominaga, Yoshinori
Journal of Heterocyclic Chemistry, 2007 , vol. 44, # 1 p. 115 - 132
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=150°C; 3 h;
参考文献
Tominaga; Sakai; Kohra; et al.
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 3 p. 962 - 970
反应条件
sodium hydroxide in dimethyl sulfoxide
T=20°C; 3 h;
参考文献
Mizuyama, Naoko; Murakami, Yuka; Kohra, Shinya; Ueda, Kazuo; Hiraoka, Kyoko; Nagaoka, Junko; Takahashi, Kojiro; Shigemitsu, Yasuhiro; Tominaga, Yoshinori
Journal of Heterocyclic Chemistry, 2007 , vol. 44, # 1 p. 115 - 132
反应条件
sodium hydroxide in dimethyl sulfoxide
T=20°C; 3 h;
参考文献
Mizuyama, Naoko; Murakami, Yuka; Kohra, Shinya; Ueda, Kazuo; Hiraoka, Kyoko; Nagaoka, Junko; Takahashi, Kojiro; Shigemitsu, Yasuhiro; Tominaga, Yoshinori
Journal of Heterocyclic Chemistry, 2007 , vol. 44, # 1 p. 115 - 132
反应条件
potassium hydroxide in N,N-dimethyl-formamide
6 h; Ambient temperature;
参考文献
Mizuyama, Naoko; Murakami, Yuka; Kohra, Shinya; Ueda, Kazuo; Hiraoka, Kyoko; Nagaoka, Junko; Takahashi, Kojiro; Shigemitsu, Yasuhiro; Tominaga, Yoshinori
Journal of Heterocyclic Chemistry, 2007 , vol. 44, # 1 p. 115 - 132
