己基(E)-3-苯基丙-2-烯酸酯合成路线 (共 4 条)
反应条件
tetrabutylammomium bromide; potassium carbonate; copper(II) sulfate; palladium dichloride in water T=85°C; Heck Reaction; 10 h; Schlenk technique; stereoselective reaction;
参考文献
Tang, Bo-Xiao; Fang, Xiao-Niu; Kuang, Ren-Yun; Hu, Rong-Hua; Wang, Ji-Wei; Li, Ping; Li, Xiao-Hang
Synthesis (Germany), 2013 , vol. 45, # 21 art. no. SS-2013-F0473-OP, p. 2971 - 2976
反应条件
bis-triphenylphosphine-palladium(II) chloride; potassium carbonate; benzyl chloride in tetrahydrofuran T=60°C; 20 h; Inert atmosphere; chemoselective reaction;
参考文献
Liu, Chao; Tang, Shan; Zheng, Liwei; Liu, Dong; Zhang, Heng; Lei, Aiwen
Angewandte Chemie - International Edition, 2012 , vol. 51, # 23 p. 5662 - 5666
参考文献
Pollard; Mattson
Journal of the American Chemical Society, 1956 , vol. 78, p. 4089
参考文献
Kailan; Hartel
Monatshefte fuer Chemie, 1937 , vol. 70, p. 329,349, 350