5-硝基-2,3,3-三甲基吲哚合成路线 （共 9 条）
反应条件
sodium nitrate; sulfuric acid T=0 - 5°C; 1 h;
参考文献
LABORATOIRES SYNTH-INNOVE
Patent: US2012/45851 A1, 2012 ;
Location in patent: Page/Page column 14; 18 ;
参考文献
Journal of the American Chemical Society, , vol. 75, p. 1877,1880
反应条件
sulfuric acid in water; acetic acid 8 h; Inert atmosphereReflux;
参考文献
Mancois, Fabien; Pozzo, Jean-Luc; Pan, Jianfeng; Adamietz, Frederic; Rodriguez, Vincent; Ducasse, Laurent; Castet, Frederic; Plaquet, Aurelie; Champagne, Benoit
Chemistry - A European Journal, 2009 , vol. 15, # 11 p. 2560 - 2571
反应条件
hydrogenchloride; acetic acid in water Fischer indole synthesis; 4 h;
参考文献
Sajjadifar, Sami; Vahedi, Hooshang; Massoudi, Abdolhossien; Louie, Omid
Molecules, 2010 , vol. 15, # 4 p. 2491 - 2498
反应条件
acetic acid Fischer indole synthesis; 1.5 h; Reflux;
参考文献
Sajjadifar, Sami; Vahedi, Hooshang; Massoudi, Abdolhossien; Louie, Omid
Molecules, 2010 , vol. 15, # 4 p. 2491 - 2498
反应条件
1: Heating 2: NaOH View Scheme
参考文献
Arakawa, Sei'ichi; Kondo, Hirofumi; Seto, Jun'etsu
Chemistry Letters, 1985 , p. 1805 - 1808
反应条件
1: With hydrogenchloride; SnCl2·2H2O in water
2 h; Reflux;
2: With sodium hydrogencarbonate in water
参考文献
LABORATOIRES SYNTH-INNOVE
Patent: US2012/45851 A1, 2012 ;
Location in patent: Page/Page column 14; 18 ;
反应条件
trifluoroacetic acid; palladium monocarbide in methanol; dichloromethane; water
参考文献
DAKO DENMARK A/S
Patent: US2011/230664 A1, 2011 ;
反应条件
1: 60 percent / iron powder, acetic acid / H2O; ethanol / 1 h / Heating
2: 33 percent / ethanol / 1.5 h / Heating
View Scheme
参考文献
Lyubich, M. S.; Isaev, Sh. G.; Al'perovich, M. A.; Shpileva, I. S.; Arshava, B. M.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1984 , vol. 20, # 9 p. 976 - 977
Khimiya Geterotsiklicheskikh Soedinenii, 1984 , vol. 20, # 9 p. 1198 - 1199
