4-硝基苯基-β-D-纤维二糖苷合成路线 （共 22 条）
反应条件
sodium methylate in methanol Ambient temperature;
参考文献
Sangseethong, Kunruedee; Penner, Michael H.
Carbohydrate Research, 1998 , vol. 314, # 3-4 p. 245 - 250
反应条件
Thermus nonproteolyticus HG102 E338A mutant; glycine; sodium hydroxide in aq. buffer T=45°C; pH=8.8; 48 h; Enzymatic reaction; pH-valueConcentrationTemperature; Overall yield = 96 percent;
参考文献
European Journal of Organic Chemistry, , # 12 p. 2414 - 2419
反应条件
AbgGlu358Ala; ammonium bicarbonate buffer 8 h; Ambient temperature;
参考文献
Journal of the American Chemical Society, , vol. 120, # 22 p. 5583 - 5584
反应条件
1: hydrogen bromide; acetic acid / dichloromethane / 0 - 20 °C 2: tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide / water; dichloromethane / 20 °C 3: methanol; sodium methylate / 20 °C / pH 10 - 11 View Scheme
参考文献
European Journal of Organic Chemistry, , # 12 p. 2414 - 2419
反应条件
1: pyridine / 20 °C 2: hydrogen bromide; acetic acid / dichloromethane / 0 - 20 °C 3: tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide / water; dichloromethane / 20 °C 4: methanol; sodium methylate / 20 °C / pH 10 - 11 View Scheme
参考文献
European Journal of Organic Chemistry, , # 12 p. 2414 - 2419
反应条件
1: methanol; sodium methylate / 20 °C 2: sodium hydroxide; Thermus nonproteolyticus HG102 E338A mutant; glycine / aq. buffer / 48 h / 45 °C / pH 8.8 / |Enzymatic reaction View Scheme
参考文献
European Journal of Organic Chemistry, , # 12 p. 2414 - 2419
反应条件
1: pyridine; hydrogen fluoride / -20 - 20 °C 2: methanol; sodium methylate / 20 °C 3: sodium hydroxide; Thermus nonproteolyticus HG102 E338A mutant; glycine / aq. buffer / 48 h / 45 °C / pH 8.8 / |Enzymatic reaction View Scheme
参考文献
European Journal of Organic Chemistry, , # 12 p. 2414 - 2419
反应条件
1: methanol; sodium methylate / 20 °C / pH 10 - 11 2: sodium hydroxide; Thermus nonproteolyticus HG102 E338A mutant; glycine / aq. buffer / 48 h / 45 °C / pH 8.8 / |Enzymatic reaction View Scheme
参考文献
European Journal of Organic Chemistry, , # 12 p. 2414 - 2419
反应条件
1: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C / |Inert atmosphere 2: methanol; sodium methylate / 20 °C / pH 10 - 11 3: sodium hydroxide; Thermus nonproteolyticus HG102 E338A mutant; glycine / aq. buffer / 48 h / 45 °C / pH 8.8 / |Enzymatic reaction View Scheme
参考文献
European Journal of Organic Chemistry, , # 12 p. 2414 - 2419
反应条件
1: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C / |Inert atmosphere 2: methanol; sodium methylate / 20 °C / pH 10 - 11 3: sodium hydroxide; Thermus nonproteolyticus HG102 E338A mutant; glycine / aq. buffer / 48 h / 45 °C / pH 8.8 / |Enzymatic reaction View Scheme
参考文献
European Journal of Organic Chemistry, , # 12 p. 2414 - 2419
