N-[4-氯-3-(三氟甲基)苯基]-乙酰胺合成路线 (共 4 条)
反应条件
1: With hydrogen fluoride; SbF5 T=-20 - 0°C; 2 h; 2: With pyridine; hydrogen fluoride T=-78 - 0°C;
参考文献
Debarge, Sebastien; Violeau, Bruno; Bendaoud, Nohair; Jacquesy, Jean-Claude
Tetrahedron Letters, 2003 , vol. 44, # 9 p. 1747 - 1750
参考文献
The State of Oregon, acting by and through The Oregon State Board of Higher Education, acting for and on behalf of The Oregon Health Sciences University; The University of Oregon; The Regents of the University of California
Patent: US5514680 A1, 1996 ;
US 5514680 A
反应条件
XeF2 in dichloromethane 2 h; Ambient temperature;
参考文献
Tanabe, Yoo; Matsuo, Noritada; Ohno, Nobuo
Journal of Organic Chemistry, 1988 , vol. 53, # 19 p. 4582 - 4585
反应条件
hydrogen; palladium on activated charcoal
参考文献
Debarge, Sebastien; Violeau, Bruno; Bendaoud, Nohair; Jacquesy, Jean-Claude
Tetrahedron Letters, 2003 , vol. 44, # 9 p. 1747 - 1750