CBZ-L-天门冬氨酸β-苄酯合成路线 （共 20 条）
反应条件
4-methyl-morpholine in water; acetonitrile T=30°C; P=7500600 Torr; 96 h;
参考文献
Yamamoto, Yoshinori; Furuta, Toshiaki; Matsuo, Jiro; Kurata, Tetsuro
Journal of Organic Chemistry, 1991 , vol. 56, # 20 p. 5737 - 5738
反应条件
sodium hydrogencarbonate in tetrahydrofuran; water T=20°C; 1 h;
参考文献
Yoshida, Masanori; Narita, Mao; Hara, Shoji
Journal of Organic Chemistry, 2011 , vol. 76, # 20 p. 8513 - 8517
反应条件
triethylamine in dichloromethane T=0°C; 1 h; Yield given. Title compound not separated from byproducts;
参考文献
Jouin, P.; Castro, B.; Zeggaf, C.; Pantaloni, A.; Senet, J.P; et al
Tetrahedron Letters, 1987 , vol. 28, # 15 p. 1665 - 1668
反应条件
triethylamine in dichloromethane T=0°C; 1 h; Yields of byproduct given;
参考文献
Jouin, P.; Castro, B.; Zeggaf, C.; Pantaloni, A.; Senet, J.P; et al
Tetrahedron Letters, 1987 , vol. 28, # 15 p. 1665 - 1668
反应条件
1: toluene 2: aqueous dioxane; aqueous NaOH View Scheme
参考文献
Journal of the American Chemical Society, , vol. 73, p. 4084,4087
反应条件
1: toluene 2: aqueous dioxane; aqueous NaOH View Scheme
参考文献
Journal of the American Chemical Society, , vol. 73, p. 4084,4087
反应条件
4-(N,N-dimethlyamino)pyridine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in dichloromethane T=0 - 20°C; 20 h; Title compound not separated from byproducts.;
参考文献
Journal of the Chemical Society, Perkin Transactions 1, , # 20 p. 3451 - 3459
反应条件
1: H2SO4 2: aq. NaHCO3 View Scheme
参考文献
Indian Journal of Chemistry, , vol. 3, p. 554 - 558
参考文献
Tetrahedron Letters, , vol. 40, # 22 p. 4275 - 4278
反应条件
1: 58 percent / camphorsulfonic acid / benzene / Heating 2: 65 percent / CF3COOH; Et3SiH / CHCl3 / 120 h 3: 65 percent / H2 / 10 percent Pd-C / ethanol / 20 °C View Scheme
参考文献
Aurelio, Luigi; Brownlee, Robert T. C.; Hughes, Andrew B.; Sleebs, Brad E.
Australian Journal of Chemistry, 2000 , vol. 53, # 5 p. 425 - 433
