2-(溴甲基)四氢-2H-吡喃合成路线 (共 16 条)
反应条件
N-bromosuccinmide; triphenylphosphine
参考文献
Gribble, Gordon W.; Silva, Richard A.; Saulnier, Mark G.
Synthetic Communications, 1999 , vol. 29, # 4 p. 729 - 747
反应条件
1: 7 percent / BrCCl3; AIBN / benzene / 80 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 45, # 29 p. 5619 - 5621
反应条件
adamantylideneadamantane bromonium triflate in 1,2-dichloro-ethane T=25°C; Rate constant;
参考文献
Canadian Journal of Chemistry, , vol. 72, # 12 p. 2540 - 2544
反应条件
bislt;(p-nitrophenyl)sulfonylgt; peroxide; 2-farnesylacetoxyethyltriethylammonium bromide in acetonitrile
参考文献
Yoshida, Masato; Mochizuki, Hideki; Suzuki, Takashi; Kamigata, Nobumasa
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 12 p. 3704 - 3706
反应条件
1: Raney nickel / Hydrogenation 2: benzene; pyridine; phosphorus (III)-bromide View Scheme
参考文献
Bulletin de la Societe Chimique de France, , p. 1254,1256
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Synthetic Communications, , vol. 22, # 15 p. 2187 - 2191
反应条件
in 1,2-dichloro-ethane T=25°C; also in the presence of adamantylideneadamoratane; Rate constant;
参考文献
Canadian Journal of Chemistry, , vol. 75, # 12 p. 1844 - 1850
反应条件
1: 59 percent / LDA / tetrahydrofuran / 0.17 h / -78 °C 2: 62 percent / lithium naphthalenide / tetrahydrofuran / 0.08 h View Scheme
参考文献
Kang, Yoon Ho; Kim, Kyongtae
Tetrahedron, 1999 , vol. 55, # 14 p. 4271 - 4286
反应条件
in dimethyl sulfoxide
参考文献
Kolb, Hartmuth C.; Cavallaro, Cullen; Shi, Zhi-Cai; Gontcharov, Alexander; Wang, Zhi-Min; Richardson, Paul F.; Kanamarlapudi, Ramanaiah C.
Patent: US2003/135050 A1, 2003 ;
反应条件
1: With sodium in diethyl ether Metallation; 2 h; Heating; 2: With water Hydrolysis;
参考文献
Tra Anh; Blancou; Commeyras
Journal of Fluorine Chemistry, 1999 , vol. 96, # 2 p. 167 - 174