4-二氮杂-N,N-二乙基苯胺氟硼酸合成路线 （共 5 条）
反应条件
hydrogenchloride; sodium nitrite in water
参考文献
Walkow, F.; Israel, G.
Journal fuer Praktische Chemie (Leipzig), 1990 , vol. 332, # 6 p. 835 - 840
反应条件
dibenzo-18-crown-6; potassium bromide; copper(ll) bromide; 1,10-phenanthroline; copper(I) bromide in acetonitrile T=20°C; Sandmeyer bromination; 0.333333 h;
参考文献
Beletskaya, Irina P.; Sigeev, Alexander S.; Peregudov, Alexander S.; Petrovskii, Pavel V.
Synthesis, 2007 , # 16 p. 2534 - 2538
反应条件
[(1,3-dimesitylimidazol-2-ylidene)(naphthoquinone)Pd(0)]2 in methanol T=50°C; Heck reaction; 1 h;
参考文献
Selvakumar, Kumaravel; Zapf, Alexander; Spannenberg, Anke; Beller, Matthias
Chemistry - A European Journal, 2002 , vol. 8, # 17 p. 3901 - 3906
反应条件
ammonium hydroxide
1.)10 deg C, 1 h 2.)r.t., 3 h;
参考文献
Traven', V. F.; Kostyuchenko, E. E.; Mkhitarov, R. A.; Men'shikova, N. F.; Oreshin, M. M.; Stepanov, B. I.
Journal of Organic Chemistry USSR (English Translation), 1980 , p. 922 - 930
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 5 p. 1047 - 1056
反应条件
[(1,3-dimesitylimidazol-2-ylidene)(naphthoquinone)Pd(0)]2 in methanol
T=50°C; Suzuki coupling; 1 h;
参考文献
Selvakumar, Kumaravel; Zapf, Alexander; Spannenberg, Anke; Beller, Matthias
Chemistry - A European Journal, 2002 , vol. 8, # 17 p. 3901 - 3906
