1: α-phenylbenzeneacetic acid With oxalyl dichloride in dichloromethane; N,N-dimethyl-formamide T=25°C; 2: methanol in dichloromethane T=25°C; Cooling with ice;
4 A molecular sieve; caesium carbonate; palladium dichloride in N,N-dimethyl-formamide T=100°C; Phenylation; 2 h;
参考文献
Satoh, Tetsuya; Inoh, Jun-Ichi; Kawamura, Yoshiki; Kawamura, Yuichiro; Miura, Masahiro; Nomura, Masakatsu
Bulletin of the Chemical Society of Japan, 1998 , vol. 71, # 9 p. 2239 - 2246
4 A molecular sieve; caesium carbonate; triphenylphosphine; palladium dichloride in N,N-dimethyl-formamide T=130°C; Phenylation; 4 h;
参考文献
Satoh, Tetsuya; Inoh, Jun-Ichi; Kawamura, Yoshiki; Kawamura, Yuichiro; Miura, Masahiro; Nomura, Masakatsu
Bulletin of the Chemical Society of Japan, 1998 , vol. 71, # 9 p. 2239 - 2246
