反应条件
1: 72 percent / K2CO3 / 5 h / 200 °C / 25857.4 Torr
2: 90 percent / K2CO3 / 2.5 h / Ambient temperature
3: 1.) NaH / 1.) DMF, 2.) DMF, overnight
4: 50percent aq. NaOH / methanol / 0.08 h / Heating
5: 56 percent / POCl3 / 4 h / Heating
6: 71 percent / m-chloroperbenzoic acid / ethanol; CHCl3 / 3 h / -40 - -30 °C
View Scheme
参考文献
Robertson; Beedle; Krushinski; Pollock; Wilson; Wyss; Hayes
Journal of Medicinal Chemistry, 1985 , vol. 28, # 6 p. 717 - 727
