(4-甲氧基苄基)三苯基氯化膦合成路线 （共 37 条）
参考文献
Armesto, Diego; Ortiz, Maria J.; Agarrabeitia, Antonia R.; Martin-Fontecha, Mar; El-Boulifi, Noureddin; Duran-Sampedro, Gonzalo; Enma, Danielle
Organic Letters, 2009 , vol. 11, # 18 p. 4148 - 4151
反应条件
1: thionyl chloride / diethyl ether / 3 h / 20 °C / |Inert atmosphere 2: toluene / 7 h / |Inert atmosphere; |Reflux View Scheme
参考文献
Tetrahedron, , vol. 69, # 13 p. 2807 - 2815
反应条件
1: n-butyl-lithium / hexane; benzene / 1 h 2: benzene / 1 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 3059 - 3064
反应条件
1: 100 percent / benzene / 24 h / Ambient temperature 2: n-butyl-lithium / hexane; benzene / 1 h 3: benzene / 1 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 3059 - 3064
反应条件
1: 100 percent / benzene / 24 h / Ambient temperature 2: n-butyl-lithium / hexane; benzene / 1 h 3: benzene / 1 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 3059 - 3064
反应条件
1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 - 20 °C / |Inert atmosphere 2: thionyl chloride / diethyl ether / 3 h / 20 °C / |Inert atmosphere 3: toluene / 7 h / |Inert atmosphere; |Reflux View Scheme
参考文献
Tetrahedron, , vol. 69, # 13 p. 2807 - 2815
反应条件
1: potassium carbonate / acetone / 4 h / |Inert atmosphere; |Reflux 2: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 - 20 °C / |Inert atmosphere 3: thionyl chloride / diethyl ether / 3 h / 20 °C / |Inert atmosphere 4: toluene / 7 h / |Inert atmosphere; |Reflux View Scheme
参考文献
Tetrahedron, , vol. 69, # 13 p. 2807 - 2815
反应条件
hydrogenchloride 12 h; Heating; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 58, # 21 p. 5643 - 5649
反应条件
in benzene 1 h; Ambient temperature;
参考文献
Zaslona, Alexander T.; Hall, C. Dennis
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 3059 - 3064
参考文献
Justus Liebigs Annalen der Chemie, , vol. 698, p. 106 - 108
