反应条件
1: 1.) lithium isopropylcyclohexylamide / 1.) THF, hexane, -78 deg C, 1 h, 2.) -78 deg C, 2 h 50 min 2: 15 percent / conc. H2SO4 / methanol / 0.08 h / -35 °C 3: 84 percent / LiAlH4 / tetrahydrofuran / 0.17 h / Ambient temperature 4: 79 percent / 8percent aq. HCl / diethyl ether 5: 47 percent / KOH / aq. ethanol / 0.58 h / Heating View Scheme
参考文献
Forbes, Craig P.; Schoeman, Wentzel J.; Strauss, Heinrich F.; Venter, Elize M. M.; Wenteler, George L.; Wiechers, Adriaan
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 906 - 910
