2-硝基-1-苯基硫基-4-(三氟甲基)苯合成路线 (共 9 条)
反应条件
ethylenediamine; copper(l) chloride in water T=120°C; 36 h; Inert atmosphere;
参考文献
Herrero, Maria Teresa; SanMartin, Raul; Dominguez, Esther
Tetrahedron, 2009 , vol. 65, # 7 p. 1500 - 1503
反应条件
tetrabutyl ammonium fluoride in acetonitrile T=25°C; 5 h; Microwave irradiation;
参考文献
Liu, Chuanzhi; Zang, Xufeng; Yu, Baohua; Yu, Xiaochun; Xu, Qing
Synlett, 2011 , # 8 art. no. W03511ST, p. 1143 - 1148
反应条件
CuSO4‵5H2O; sodium carbonate; sodium L-ascorbate; L-proline in water; dimethyl sulfoxide T=70°C; 12 h;
参考文献
Goriya, Yogesh; Ramana
Tetrahedron, 2010 , vol. 66, # 38 p. 7642 - 7650
反应条件
copper(l) iodide; (1S,2S)-1,2-diaminocyclohexane in water T=120°C;
参考文献
Carril, Monica; SanMartin, Raul; Dominguez, Esther; Tellitu, Imanol
Chemistry - A European Journal, 2007 , vol. 13, # 18 p. 5100 - 5105
反应条件
potassium hydroxide in ethanol; water
参考文献
Hoffmann-La Roche Inc.
Patent: US4006144 A1, 1977 ;
参考文献
Bunnett; Davis
Journal of the American Chemical Society, 1954 , vol. 76, p. 3011,3013
Full Text Show Details
Stacy et al.
Journal of Organic Chemistry, 1957 , vol. 22, p. 298,299, 301
反应条件
isopropyl-benzene; triethyl phosphite Heating;
参考文献
Cadogan,J.I.G. et al.
Journal of the Chemical Society [Section] C: Organic, 1970 , p. 2437 - 2441
反应条件
dihydrogen peroxide; acetic acid
参考文献
Stacy et al.
Journal of Organic Chemistry, 1957 , vol. 22, p. 298,299, 301
反应条件
1: aqueous H2O2; acetic acid
2: Raney nickel / Hydrogenation
View Scheme
参考文献
Stacy et al.
Journal of Organic Chemistry, 1957 , vol. 22, p. 298,299, 301