(S)-(+)-3-喹宁醇合成路线 （共 15 条）
反应条件
RuCl[(S)-daipena][(S)-3,5-xylyl-BINAP]; potassium tert-butylate; hydrogen in isopropyl alcohol T=10°C; P=22801.5 Torr; 6 h; optical yield given as percent eeenantioselective reaction;
参考文献
Matsumura, Kazuhiko; Arai, Noriyoshi; Hori, Kiyoto; Saito, Takao; Sayo, Noboru; Ohkuma, Takeshi
Journal of the American Chemical Society, 2011 , vol. 133, # 28 p. 10696 - 10699
反应条件
D-glucose in aq. phosphate buffer T=30°C; pH=8; 48 h; ConcentrationTemperaturepH-valueTime;
参考文献
Wang, Yu; Li, Jianjiong; Wu, Qiaqing; Zhu, Dunming
Journal of Molecular Catalysis B: Enzymatic, 2013 , vol. 88, p. 14 - 19
反应条件
hydrogen; (S)-1-[(R)-1',2- bis (diphenylphosphino) ferrocenyl] ethanol; 1,5-cyclooctadienerhodium (I) chloride dimer; (1R,2R)-(+)-1,2-diphenylethylenediamine in ethanol T=30°C; P=26252.6 Torr; 16 h; Product distribution / selectivity;
参考文献
WO2004/78686 A1, ;
Page 14, 15 ;
反应条件
camphor-10-sulfonic acid
参考文献
Journal of the American Chemical Society, , vol. 74, p. 2219
反应条件
potassium hydroxide; ethanol T=20°C; 0.5 h;
参考文献
WO2007/93602 A1, ;
Page/Page column 16 ;
参考文献
Lonza AG
Patent: US5744606 A1, 1998 ;
反应条件
H2 in hydrogenchloride; methanol; dichloromethane
反应条件
Aspergillus melleus protease in phosphate buffer T=25°C; pH=7.5; 16 h; Title compound not separated from byproducts;
参考文献
Tetrahedron Asymmetry, , vol. 14, # 13 p. 1871 - 1877
反应条件
1: potassium; toluene / anschliessend mit konz. Salzsaeure 2: lithium alanate; diethyl ether 3: (1S)-2-oxo-bornane-10-sulfonic acid View Scheme
参考文献
Journal of the American Chemical Society, , vol. 74, p. 2219
反应条件
sodium hydroxide T=50°C; 1 h;
参考文献
Synthetic Communications, , vol. 22, # 13 p. 1895 - 1911
