4,4'-二甲基苯偶酰合成路线 （共 111 条）
反应条件
aluminium trichloride 1.) RT, 2.5 h, 2.) reflux, 0.5 h;
参考文献
Journal of the American Chemical Society, , vol. 112, # 8 p. 3068 - 3082
反应条件
formic acid; sulfuric acid 0.05 h; microwave irradiation;
参考文献
Rao, H. Surya Prakash; Jothilingam; Vasantham; Scheeren, Hans W.
Tetrahedron Letters, 2007 , vol. 48, # 26 p. 4495 - 4497
反应条件
1: 70 percent / SmI2 / tetrahydrofuran / 18.5 h / Heating 2: HCl / 14 h View Scheme
参考文献
Chemistry Letters, , vol. 33, # 2 p. 102 - 103
反应条件
1: tetrahydrofuran / 0.33 h / -40 °C 2: SmI2 / tetrahydrofuran / 0.08 h / -40 °C View Scheme
参考文献
Chemical Communications, , # 23 p. 2307 - 2308
反应条件
amalgamated magnesium; titanium tetrachloride in tetrahydrofuran 0 deg C -> room temperature, 2 h;
参考文献
Synthetic Communications, , vol. 19, # 11-12 p. 2159 - 2166
反应条件
in ethylene glycol T=180°C; 1 h;
参考文献
Lee, Chang Kiu; Kim, Sun Hee; Kim, Yong Bun
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 4 p. 1019 - 1024
反应条件
Grubb's 2nd generation catalyst; tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide in water; toluene; acetonitrile T=20°C; 1 h; Inert atmosphere;
参考文献
Schmidt, Bernd; Krehl, Stefan; Hauke, Sylvia
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5427 - 5435
反应条件
TDBPA(1+)*SbCl6(1-) in dichloromethane 0.25 h; Ambient temperature;
参考文献
Lopez, Luigi; Mele, Giuseppe; Nacci, Angelo; Troisi, Luigino
Tetrahedron Letters, 1993 , vol. 34, # 24 p. 3897 - 3900
反应条件
zinc; palladium diacetate in acetone 1 h; Ambient temperature;
参考文献
Chemistry Letters, , p. 1201 - 1202
反应条件
dimethyl sulfoxide 0.05 h; Irradiation;
参考文献
Villemin; Hammadi
Synthetic Communications, 1995 , vol. 25, # 20 p. 3145 - 3148
