(2-氧代-2-苯乙基)膦酸二乙酯合成路线 (共 61 条)
反应条件
1: (i) Na, (ii) /BRN= 606222/ 2: aq. EtOH, H2SO4 / HgSO4 View Scheme
参考文献
Bulletin de la Societe Chimique de France, , p. 1707 - 1713
反应条件
magnesium chloride in toluene 12 h; Ambient temperature; Yield given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 9 p. 1360 - 1364
反应条件
n-butyllithium; lithium hexamethyldisilazane Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 51, # 23 p. 4342 - 4347
参考文献
Tetrahedron Letters, , vol. 42, # 26 p. 4365 - 4368
Russian Journal of General Chemistry, , vol. 73, # 11 p. 1729 - 1737
反应条件
diethyl cyanophosphonate; benzotriazol-1-ol; triethylamine; trifluoroacetic acid; Wang resin; diisopropyl-carbodiimide 1.) DMF, 0 deg C; 2.) DMF; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 39, # 15 p. 2195 - 2198
反应条件
1: 1) MgCl2, Et3N / 1) CH2Cl2, room temperature, 30 min, 2) 20 deg C 2: H2O / 2.5 h / Heating View Scheme
参考文献
Synthetic Communications, , vol. 26, # 13 p. 2561 - 2568
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , p. 604 - 610
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 675 - 683
反应条件
in toluene Michaelis-Arbuzov Synthesis; 2 h; Dean-StarkReflux;
参考文献
Journal of Organic Chemistry, , vol. 78, # 17 p. 8232 - 8241
反应条件
(i) nBuLi, THF, hexane, (ii) /BRN= 1072099/; Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 37, p. 939 - 943
反应条件
Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 56, # 19 p. 5556 - 5560