(2-氧代-2-苯乙基)膦酸二乙酯合成路线 （共 61 条）
反应条件
water; palladium dichloride in 1,4-dioxane T=80°C; 2 h;
参考文献
Li, Xiubin; Hu, Gaobo; Luo, Ping; Tang, Guo; Gao, Yuxing; Xu, Pengxiang; Zhao, Yufen
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 13 p. 2427 - 2432
反应条件
1: methyl phosphonic acid,diethyl ester With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.333333 h; 2: With copper(I) bromide in tetrahydrofuran; hexane T=-60 - -30°C; 1.5 h; 3: benzoyl chloride in tetrahydrofuran; hexane T=-40 - -30°C; Further stages.;
参考文献
Nesterov; Kolodiazhnyi
Tetrahedron, 2007 , vol. 63, # 29 p. 6720 - 6731
反应条件
triethylamine; magnesium chloride in acetonitrile T=20°C; Acylation; 15 h;
参考文献
Corbel, Bernard; L'Hostis-Kervella, Isabelle; Haelters, Jean-Pierre
Synthetic Communications, 2000 , vol. 30, # 4 p. 609 - 618
反应条件
magnesium; trimethylphosphane; CoCl2 in tetrahydrofuran T=20°C;
参考文献
Orsini, Fulvia; Di Teodoro, Emanuela; Ferrari, Marinella
Synthesis, 2002 , # 12 p. 1683 - 1688
反应条件
lithium hexamethyldisilazane in tetrahydrofuran Barbier reaction; Cooling with iceInert atmosphere;
参考文献
Milburn, Robert R.; McRae, Ken; Chan, Johann; Tedrow, Jason; Larsen, Robert; Faul, Margaret
Tetrahedron Letters, 2009 , vol. 50, # 8 p. 870 - 872
反应条件
n-butyllithium; lithium diisopropyl amide in tetrahydrofuran; hexane T=-60°C;
参考文献
Aboujaoude, Elie Elia; Collignon, Noel; Teulade, Marie-Paule; Savignac, Philippe
Phosphorus and Sulfur and the Related Elements, 1985 , vol. 25, p. 57 - 62
反应条件
iodosylbenzene; boron trifluoride diethyl etherate in dichloromethane T=-40 - 20°C; 2.5 h;
参考文献
Dae Young Kim; Joo Yang Mang; Dong Young Oh
Synthetic Communications, 1994 , vol. 24, # 5 p. 629 - 634
反应条件
iron tribromide; oxygen; triethylamine; copper(ll) bromide in dimethyl sulfoxide T=55°C; 24 h;
参考文献
Wei, Wei; Ji, Jian-Xin
Angewandte Chemie - International Edition, 2011 , vol. 50, # 39 p. 9097 - 9099
反应条件
lithium hexamethyldisilazane in tetrahydrofuran Barbier reaction; Cooling with iceInert atmosphere;
参考文献
Milburn, Robert R.; McRae, Ken; Chan, Johann; Tedrow, Jason; Larsen, Robert; Faul, Margaret
Tetrahedron Letters, 2009 , vol. 50, # 8 p. 870 - 872
反应条件
samarium diiodide in tetrahydrofuran T=20°C; 12 h;
参考文献
Tetrahedron Letters, , vol. 43, # 40 p. 7259 - 7261
