4,4'-二氟二苯甲酮合成路线 (共 115 条)
反应条件
CaY zeolite in hexane 3 h; Ambient temperature; Yield givenYields of byproduct given;
参考文献
Journal of Physical Chemistry A, , vol. 102, # 28 p. 5627 - 5638
反应条件
1: p-TsOH / benzene / Heating 2: Ca zeolite / hexane / 3 h / Ambient temperature View Scheme
参考文献
Journal of Physical Chemistry A, , vol. 102, # 28 p. 5627 - 5638
反应条件
antimony(V) pentachloride; SbF3 T=160°C;
参考文献
Journal of the Chemical Society, , p. 4710,4712
反应条件
in tetrahydrofuran T=-70 - 20°C; 6 h;
参考文献
WO2004/24663 A1, ;
Page/Page column 12 ;
反应条件
air; acetic acid T=23°C; 12 h; Further byproducts given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 64, # 6 p. 1800 - 1809
反应条件
n-butyllithium; water; iodine 1.) THF, -78 deg C, 10 min, 2.) THF, -78 deg C, 20 min, 3.) -78 deg C to room temperature; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 63, # 5 p. 1467 - 1472
反应条件
1: With aluminium trichloride; iron(III) chloride 2: in water
参考文献
Russian Chemical Bulletin, , vol. 50, # 7 p. 1208 - 1213
反应条件
1: 21 percent / HNO3, H2SO4 / 2 h / 50 °C 2: 59 percent / (CH3)4NF, CH3CON(CH3)2 / 1 h / 100 °C View Scheme
参考文献
Journal of Fluorine Chemistry, , vol. 92, # 2 p. 127 - 129
反应条件
1: CS2; AlCl3 2: aqueous ethanol View Scheme
参考文献
Journal of the Chemical Society, , p. 4710,4712
参考文献
Journal of the Chemical Society, , p. 4710,4712