1-[4-(2-氟苯基)苯基]乙酮合成路线 (共 6 条)
反应条件
sodium hypobromide in 1,4-dioxane
参考文献
Byron,D.J. et al.
Journal of the Chemical Society [Section] C: Organic, 1966 , p. 840 - 845
反应条件
air; potassium carbonate; oxime-based palladacycle/polyvinylpyridine in toluene
T=110°C; Suzuki-Miyaura cross-coupling reaction; 2 h;
参考文献
Solodenko, Wladimir; Mennecke, Klaas; Vogt, Carla; Gruhl, Susan; Kirschning, Andreas
Synthesis, 2006 , # 11 p. 1873 - 1881
反应条件
aluminium trichloride in dichloromethane
10 h; Ambient temperature;
参考文献
Thompson, Neil J.; Goodby, John W.; Toyne, Kenneth J.
Molecular Crystals and Liquid Crystals Science and Technology, Section A: Molecular Crystals and Liquid Crystals, 1992 , vol. 214, p. 81 - 96
反应条件
1: 2-fluoro-biphenyl With AlCl3, aluminium chloride in carbon disulfide
0.0833333 h; Reflux;
2: acetic anhydride in carbon disulfide
2 h; Reflux;
参考文献
Kourounakis, Angeliki P.; Charitos, Christos; Rekka, Eleni A.; Kourounakis, Panos N.
Journal of Medicinal Chemistry, 2008 , vol. 51, # 18 p. 5861 - 5865
反应条件
nickel kieselguhr; 2-methyl cyclohexane
T=125 - 150°C; P=102971 Torr; Hydrogenation;
参考文献
Renoll
Journal of the American Chemical Society, 1946 , vol. 68, p. 1159
反应条件
T=125 - 130°C; P=102971 Torr; Hydrogenation;
参考文献
Renoll
Journal of the American Chemical Society, 1946 , vol. 68, p. 1159