4,4’-双[(4-溴苯基)苯氨基]联苯合成路线 (共 3 条)
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate in toluene T=90°C; Buchwald-Hartwig reaction; Inert atmosphere;
参考文献
Lim, Younhee; Park, Young-Seo; Kang, Yerang; Jang, Do Young; Kim, Joo Hyun; Kim, Jang-Joo; Sellinger, Alan; Yoon, Do Y.
Journal of the American Chemical Society, 2011 , vol. 133, # 5 p. 1375 - 1382
反应条件
1: tris-(dibenzylideneacetone)dipalladium(0); 1,1'-bis-(diphenylphosphino)ferrocene; sodium t-butanolate / toluene / 24 h / 80 °C / Inert atmosphere 2: tris-(dibenzylideneacetone)dipalladium(0); 1,1'-bis-(diphenylphosphino)ferrocene; sodium t-butanolate / toluene / 90 °C / Inert atmosphere View Scheme
参考文献
Journal of the American Chemical Society, , vol. 133, # 5 p. 1375 - 1382
反应条件
1: tris-(dibenzylideneacetone)dipalladium(0); 1,1'-bis-(diphenylphosphino)ferrocene; sodium t-butanolate / toluene / 24 h / 80 °C / Inert atmosphere 2: tris-(dibenzylideneacetone)dipalladium(0); 1,1'-bis-(diphenylphosphino)ferrocene; sodium t-butanolate / toluene / 90 °C / Inert atmosphere View Scheme
参考文献
Journal of the American Chemical Society, , vol. 133, # 5 p. 1375 - 1382