3-氧代-3-苯基丙酰胺合成路线 (共 38 条)
反应条件
Rhodococcus rhodochrous IFO 15564 in phosphate buffer; ethanol T=28°C; pH=8.0; 0.666667 h;
参考文献
Gotor, Vicente; Liz, Ramon; Testera, Ana Ma
Tetrahedron, 2004 , vol. 60, # 3 p. 607 - 618
反应条件
ammonia in 1,4-dioxane T=30°C; 68 h; Candida antarctica lipase;
参考文献
Garcia; Rebolledo; Gotor
Tetrahedron, 1994 , vol. 50, # 23 p. 6935 - 6940
反应条件
ammonia in xylene T=115°C;
参考文献
Sato, Masayuki; Ogasawara, Hiromichi; Komatsu, Sachiko; Kato, Tetsuzo
Chemical & Pharmaceutical Bulletin, 1984 , vol. 32, # 10 p. 3848 - 3856
反应条件
in water; acetonitrile T=25°C; Equilibrium constant;
参考文献
Bunting, John W.; Kanter, James P.
Journal of the American Chemical Society, 1993 , vol. 115, # 25 p. 11705 - 11715
反应条件
n-butyllithium THF, 1) 0 deg C, 30 min, 2) 0 deg C, 2h; Yield given. Multistep reaction;
参考文献
Kuzma, Peter C.; Brown, Lawrence E.; Harris, Thomas M.
Journal of Organic Chemistry, 1984 , vol. 49, # 11 p. 2015 - 2018
反应条件
n-butyllithium THF, 1) 0 deg C, 30 min, 2) 0 deg C, 3h; Yield given. Multistep reaction;
参考文献
Kuzma, Peter C.; Brown, Lawrence E.; Harris, Thomas M.
Journal of Organic Chemistry, 1984 , vol. 49, # 11 p. 2015 - 2018
参考文献
Moureu; Lazennec
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1907 , vol. 144, p. 806
Bulletin de la Societe Chimique de France, 1907 , vol. <4> 1, p. 1070
反应条件
1: alcohol 2: concentrated sulfuric acid View Scheme
参考文献
Dornow; Kuehlcke; Baxmann
Chemische Berichte, 1949 , vol. 82, p. 254,255
参考文献
Takeda,A. et al.
Bulletin of the Chemical Society of Japan, 1974 , vol. 47, p. 2440 - 2443
反应条件
hydrogenchloride; ethanol
参考文献
Dornow; Kuehlcke; Baxmann
Chemische Berichte, 1949 , vol. 82, p. 254,255