4-氯-5-甲基苯-1,3-二醇合成路线 （共 6 条）
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran 3 h; Heating;
参考文献
Mori, Kenji; Sato, Kazuo
Tetrahedron, 1982 , vol. 38, # 9 p. 1221 - 1225
反应条件
potassium hydroxide 1 h; Heating;
参考文献
Mahandru, M. Mohan; Tajbakhsh, Alireza
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 2 p. 413 - 416
反应条件
1: 29.8 g / SO2Cl2 / CH2Cl2 / 2.75 h / Heating 2: 14.3 g / NaOH (aq) / 3.5 h / Heating View Scheme
参考文献
Sala, Tony; Sargent, Melvyn V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 855 - 869
反应条件
1: 63 percent / sulphuryl chloride / diethyl ether / 1.) room temperature, 1 h, 2.) reflux, 45 min 2: 81 percent / 5percent aq. potassium hydroxide / 1 h / Heating View Scheme
参考文献
Mahandru, M. Mohan; Tajbakhsh, Alireza
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 2 p. 413 - 416
反应条件
sulfuryl dichloride; diethyl ether
参考文献
Sundholm,E.G.
Tetrahedron, 1978 , vol. 34, p. 577 - 586
反应条件
sodium hydroxide 3.5 h; Heating;
参考文献
Sala, Tony; Sargent, Melvyn V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 855 - 869
