4-溴-5-甲基苯-1,3-二醇合成路线 （共 7 条）
反应条件
tetra-n-butylammonium tribromide in methanol; dichloromethane 0.5 h; Ambient temperaturereagent 1.0 equivalent;
参考文献
Liang, Dong; Luo, Huan; Liu, Yan-Fei; Hao, Zhi-You; Wang, Yan; Zhang, Chun-Lei; Zhang, Qing-Jian; Chen, Ruo-Yun; Yu, De-Quan
Tetrahedron, 2013 , vol. 69, # 9 p. 2093 - 2097
反应条件
in diphenylether heating to 170-174 deg C during 1 h;
参考文献
Chandrasekharan, V.; Unnikrishnan, P.; Shah, G. D.; Bhattacharyya, S. C.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 12 p. 1052 - 1055
参考文献
Chakravarti; Mukerjee
Journal of the Indian Chemical Society, 1937 , vol. 14, p. 725,731
参考文献
Chakravarti; Mukerjee
Journal of the Indian Chemical Society, 1937 , vol. 14, p. 725,731
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Lamparter
Justus Liebigs Annalen der Chemie, 1865 , vol. 134, p. 247
反应条件
potassium carbonate in acetone T=20°C; 24 h;
参考文献
Hamad Elgazwy, Abdel-Sattar S.
Phosphorus, Sulfur and Silicon and Related Elements, 2000 , vol. 164, p. 131 - 143
反应条件
sodium hydroxide auf dem Dampfbad;
参考文献
Asahina; Fuzikawa
Chemische Berichte, 1934 , vol. 67, p. 163,166, 715
Yakugaku Zasshi, 1934 , vol. 54, p. 223,228
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; palladium diacetate; caesium carbonate in 1,4-dioxane; water
T=80°C; Suzuki Coupling; 3 h; Inert atmosphere;
参考文献
Liang, Dong; Luo, Huan; Liu, Yan-Fei; Hao, Zhi-You; Wang, Yan; Zhang, Chun-Lei; Zhang, Qing-Jian; Chen, Ruo-Yun; Yu, De-Quan
Tetrahedron, 2013 , vol. 69, # 9 p. 2093 - 2097
