1,4,8-三羟基-2-甲基蒽-9,10-二酮合成路线 （共 24 条）
反应条件
sulfuric acid; boric acid T=130 - 140°C; 2 h;
参考文献
Gorelik, M. V.; Arinich, L. V.; Kotlyarevskii, O. I.; Fes'kova, E. A.
Journal of Organic Chemistry USSR (English Translation), 1986 , p. 129 - 138
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 1 p. 147 - 156
反应条件
hydrogen bromide in acetic acid Heating;
参考文献
Wiseman, John R.; Pendery, John J.; Otto, Charlotte A.; Chiong, Kaolin G.
Journal of Organic Chemistry, 1980 , vol. 45, # 3 p. 516 - 519
反应条件
sodium methylate in methanol Heating;
参考文献
Cameron, Donald W.; Griffiths, Peter G.; Leung Brenda K. Y.
Tetrahedron Letters, 1995 , vol. 36, # 21 p. 3729 - 3730
反应条件
in benzene 32 h; Ambient temperature;
参考文献
Simoneau; Brassard
Tetrahedron, 1988 , vol. 44, # 4 p. 1015 - 1022
反应条件
lead dioxide in acetonitrile 288 h; Heating;
参考文献
Cano, Pilar; Echavarren, Antonio; Prados, Pilar
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5373 - 5376
反应条件
1: NaI / acetone / 31 h / Heating 2: 95 percent / zinc dust, sodium acetate 3: 1.) chromium trioxide, conc. sulfuric acid, 2.) 6 N HCl 4: 51 percent / 48percent HBr / acetic acid / Heating View Scheme
参考文献
Wiseman, John R.; Pendery, John J.; Otto, Charlotte A.; Chiong, Kaolin G.
Journal of Organic Chemistry, 1980 , vol. 45, # 3 p. 516 - 519
反应条件
1: 95 percent / zinc dust, sodium acetate 2: 1.) chromium trioxide, conc. sulfuric acid, 2.) 6 N HCl 3: 51 percent / 48percent HBr / acetic acid / Heating View Scheme
参考文献
Wiseman, John R.; Pendery, John J.; Otto, Charlotte A.; Chiong, Kaolin G.
Journal of Organic Chemistry, 1980 , vol. 45, # 3 p. 516 - 519
反应条件
1: 1.) chromium trioxide, conc. sulfuric acid, 2.) 6 N HCl 2: 51 percent / 48percent HBr / acetic acid / Heating View Scheme
参考文献
Wiseman, John R.; Pendery, John J.; Otto, Charlotte A.; Chiong, Kaolin G.
Journal of Organic Chemistry, 1980 , vol. 45, # 3 p. 516 - 519
反应条件
1: 45 percent / potassium carbonate / dimethylsulfoxide / 1 h / 20 °C 2: 85 percent / K2CO3 / acetone / 4 h / Heating 3: 78.5 percent / KOH, sulfamic acid / 9 h / Heating 4: 93 percent / conc. H2SO4, boric acid / 2 h / 130 - 140 °C View Scheme
参考文献
Gorelik, M. V.; Arinich, L. V.; Kotlyarevskii, O. I.; Fes'kova, E. A.
Journal of Organic Chemistry USSR (English Translation), 1986 , p. 129 - 138
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 1 p. 147 - 156
反应条件
1: 85 percent / K2CO3 / acetone / 4 h / Heating 2: 78.5 percent / KOH, sulfamic acid / 9 h / Heating 3: 93 percent / conc. H2SO4, boric acid / 2 h / 130 - 140 °C View Scheme
参考文献
Gorelik, M. V.; Arinich, L. V.; Kotlyarevskii, O. I.; Fes'kova, E. A.
Journal of Organic Chemistry USSR (English Translation), 1986 , p. 129 - 138
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 1 p. 147 - 156
