chlorine

1.1: hydrogenchloride; calcium chloride; sodium hypochlorite / dichloromethane; water / 0.25 h / -30 - -25 °C 1.2: 0.5 h / 0 °C / |Cooling with acetone-dry ice 2.1: N-chloro-succinimide; oxygen; copper dichloride / acetonitrile / 16 h / 130 °C / 760.05 Torr 3.1: magnesium / methanol / 20 °C / |Sonication View Scheme

1.1: hydrogenchloride; calcium chloride; sodium hypochlorite / dichloromethane; water / 0.25 h / -30 - -25 °C 1.2: 0.5 h / 0 °C / |Cooling with acetone-dry ice 2.1: N-chloro-succinimide; oxygen; copper dichloride / acetonitrile / 16 h / 130 °C / 760.05 Torr 3.1: magnesium / methanol / 20 °C / |Sonication View Scheme

potassium hydroxide

1: With tert.-butylnitrite; boron trifluoride diethyl etherate in tetrahydrofuran; dichloromethane T=-15 - 5°C; 0.5 h; 2: With hydrogenchloride; sulfur dioxide; acetic acid; copper dichloride in water; acetonitrile T=20°C; 0.5 h;

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