D-(+)-核糖酸-gamma-内酯合成路线 (共 68 条)
反应条件
hydrogen; palladium on activated charcoal in methanol T=20°C; 24 h;
参考文献
Miranda, Pedro O.; Estevez, Francisco; Quintana, Jose; Garcia, Candelaria I.; Brouard, Ignacio; Padron, Juan I.; Pivel, Juan P.; Bermejo, Jaime
Journal of Medicinal Chemistry, 2004 , vol. 47, # 2 p. 292 - 295
反应条件
bromine in water T=25°C; 120 h;
参考文献
Scarpi, Dina; Bartali, Laura; Casini, Andrea; Occhiato, Ernesto G.
European Journal of Organic Chemistry, 2013 , # 7 p. 1306 - 1317
反应条件
trifluoroacetic acid in water 2 h; Ambient temperature;
参考文献
Kozikowski,, Alan P.; Ghosh, Arun K.
Journal of Organic Chemistry, 1984 , vol. 49, # 15 p. 2762 - 2772
反应条件
trifluoroacetic acid in chloroform; water T=70°C; 10 h;
参考文献
Salas-Reyes
Synthetic Communications, 1999 , vol. 29, # 12 p. 2187 - 2199
反应条件
[Rh(H)(PEt3)3]; 4-phenylbut-3-en-2-one in N,N-dimethyl-formamide T=40°C; 4 h;
参考文献
Isaac, Isabelle; Stasik, Imane; Beaupere, Daniel; Uzan, Raoul
Tetrahedron Letters, 1995 , vol. 36, # 3 p. 383 - 386
反应条件
trifluoroacetic acid in tetrahydrofuran
参考文献
Mikami, Koichi; Terada, Masahiro; Nakai, Takeshi
Tetrahedron: Asymmetry, 1991 , vol. 2, # 10 p. 993 - 996
反应条件
1: 98 percent / aq. HCl / 7 h / Ambient temperature 2: 1.) NaH 3: 93 percent / n-Bu3SnH, AIBN / toluene / Heating 4: 96 percent / TFA / H2O; CHCl3 / 10 h / 70 °C View Scheme
参考文献
Synthetic Communications, , vol. 29, # 12 p. 2187 - 2199
反应条件
1: 1.) 10percent sodium hydroxide / 1.) EtOH 2: trifluoroacetic acid / H2O View Scheme
参考文献
Journal of the American Chemical Society, , vol. 104, # 21 p. 5788 - 5789
反应条件
bromine in water 96 h; Ambient temperature;
参考文献
Han, So-Yeop; Joullie, Madeleine M.; Petasis, Nicos A.; Bigorra, Joaquim; Corbera, Jordi; et al.
Tetrahedron, 1993 , vol. 49, # 2 p. 349 - 362
反应条件
in methanol 15 h; Irradiation;
参考文献
Chemistry - A European Journal, , vol. 6, # 22 p. 4163 - 4169