3-甲氧基-(16B,17B)-雌甾-1,3,5(10)-三烯-16,17-二醇合成路线 (共 14 条)
反应条件
potassium carbonate in ethanol; water 6 h; Heating;
参考文献
Ponsold, K.; Grosse, P.
Journal fuer Praktische Chemie (Leipzig), 1981 , vol. 323, # 5 p. 801 - 818
反应条件
air; water in N,N-dimethyl-formamide T=27°C; 48 h; Streptomyces roseochromogenes ATCC 13400; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Ferrer; Calzada; Bonet
Steroids, 1990 , vol. 55, # 9 p. 390 - 394
反应条件
tetrahydrofuran; lithium aluminium tetrahydride
参考文献
Sheehan et al.
Journal of the American Chemical Society, 1953 , vol. 75, p. 6231,6233
Journal of the American Chemical Society, 1957 , vol. 79, p. 147
参考文献
Huffman
Journal of the American Chemical Society, 1942 , vol. 64, p. 2235
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Huffman; Darby
Journal of the American Chemical Society, 1944 , vol. 66, p. 150,151
反应条件
potassium hydroxide in ethanol 0.75 h; Heating; Further byproducts given;
参考文献
Ponsold, K.; Grosse, P.
Journal fuer Praktische Chemie (Leipzig), 1981 , vol. 323, # 5 p. 801 - 818
反应条件
1: sodium; liquid NH3; diethyl ether 2: NaBH4; methanol View Scheme
参考文献
Sheehan et al.
Journal of the American Chemical Society, 1953 , vol. 75, p. 6231,6233
Journal of the American Chemical Society, 1957 , vol. 79, p. 147
反应条件
methanol; sodium tetrahydroborate
参考文献
Sheehan et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 147,148
反应条件
potassium hydroxide in ethanol 0.75 h; Heating; Further byproducts given;
参考文献
Ponsold, K.; Grosse, P.
Journal fuer Praktische Chemie (Leipzig), 1981 , vol. 323, # 5 p. 801 - 818
反应条件
1: 78 percent / acetone / 1 h 2: 3 percent / 3percent KOH / ethanol / 0.75 h / Heating View Scheme
参考文献
Ponsold, K.; Grosse, P.
Journal fuer Praktische Chemie (Leipzig), 1981 , vol. 323, # 5 p. 801 - 818
反应条件
potassium hydroxide in ethanol 0.75 h; Heating; Further byproducts given. Title compound not separated from byproducts;
参考文献
Ponsold, K.; Grosse, P.
Journal fuer Praktische Chemie (Leipzig), 1981 , vol. 323, # 5 p. 801 - 818