1: 5-Bromo-2-methyl-pyridine With n-butyllithium in diethyl ether; hexane T=-78°C; 1 h; 2: tributyltin chloride in diethyl ether; hexane T=-78 - 0°C; 1 h; 3: With water; ammonium chloride in diethyl ether; hexane
参考文献
DeGoey, David A.; Flentge, Charles A.; Flosi, William J.; Grampovnik, David J.; Kempf, Dale J.; Klein, Larry L.
Patent: US2005/131017 A1, 2005 ;
Location in patent: Page/Page column 136 ;