(1S,2R)-(+)-反-2-苯基-1-环己醇合成路线 （共 48 条）
反应条件
hydrogen; palladium on activated charcoal in methanol 4 h;
参考文献
Cravotto; Giovenzana; Pilati; Sisti; Palmisano
Journal of Organic Chemistry, 2001 , vol. 66, # 25 p. 8447 - 8453
反应条件
1: bromobenzene; magnesium With iodine in diethyl ether T=0°C; 2.5 h; Inert atmosphere; 2: copper(l) iodide; cyclohexane-1,2-epoxide in diethyl ether T=20°C; Inert atmosphere;
参考文献
Balamurugan, Rengarajan; Gudla, Vanajakshi
Organic Letters, 2009 , vol. 11, # 14 p. 3116 - 3119
反应条件
(1S,4S)-4-Bn-1-nBu-AZADOH; sodium hydrogencarbonate in dichloromethane T=-40°C; 3 h; Resolution of racemateInert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Organic Letters, , vol. 11, # 8 p. 1828 - 1831
反应条件
magnesium in tetrahydrofuran
参考文献
Eastman Kodak Company
Patent: US5312950 A1, 1994 ;
反应条件
tertiary amine-based nucleophilic catalyst in 1,1-dimethylpropan-1-ol T=0°C; 2 h;
参考文献
Chemistry Letters, , # 11 p. 1114 - 1115
反应条件
platinum(IV) oxide; hydrogen; acetic acid T=60°C; P=15001.5 Torr; 4 h; Autoclave; optical yield given as percent de;
参考文献
Sukhorukov, Alexey Yu.; Boyko, Yaroslav D.; Nelyubina, Yulia V.; Gerard, Stephane; Ioffe, Sema L.; Tartakovsky, Vladimir A.
Journal of Organic Chemistry, 2012 , vol. 77, # 12 p. 5465 - 5469
反应条件
(S,S)(4-JandaJel-CH2-O(CH2)3O)-2(BnN(Me)CH2)N(Me)pyrrolidine; 4 A molecular sieve; triethylamine in dichloromethane T=-78°C; 11 h;
参考文献
Clapham; Cho; Janda
Journal of Organic Chemistry, 2001 , vol. 66, # 3 p. 868 - 873
反应条件
(S)-HBTM; N-ethyl-N,N-diisopropylamine in 1,1-dimethylpropan-1-ol; toluene T=-40°C; 10 h; optical yield given as percent ee;
参考文献
Organic Letters, , vol. 10, # 6 p. 1115 - 1118
反应条件
1: With hydrogen in methanol T=70 - 75°C; P=30003 Torr; 5.5 h; Autoclave; 2: With dimethyl sulfoxide 0.5 h; RefluxInert atmosphere;
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 46 p. 8082 - 8091
反应条件
via enzymatic Pseudomonas sp. acyl transfer;
参考文献
Journal of the Chemical Society, Chemical Communications, , # l p. 49 - 51
