苯基 2,3,4,5-四-O-乙酰基-alpha-D-吡喃葡萄糖苷合成路线 (共 20 条)
反应条件
zinc(II) chloride T=120 - 125°C; P=30 Torr; var. reagents, var. temperature; Product distribution;
参考文献
Sokolov, V. M.; Studentsov, E. P.; Brykova, G. A.; Ivanov, M. A.; Zakharov, V. I.; Sochilin, E. G.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 6 p. 1401 - 1405,1141 - 1145
反应条件
trichlorophosphate T=55°C; 5 h; anomerisation;
参考文献
Bhat, V. S.; Sinha, Bharati; Bose, J. L.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 514 - 516
反应条件
Behandeln des Reaktionsprodukts mit Acetanhydrid und Pyridin;
参考文献
de Pascual Teresa
Anales de la Real Sociedad Espanola de Fisica y Quimica, 1954 , vol. <B> 50, p. 79,85
反应条件
pyridine; acetic anhydride 1.) CH2Cl2, reflux, 2 h, 2.) room temperature, 24 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Gurudutt, Kambadoor N.; Rao, Lingamallu Jagan Mohan; Rao, Sanjay; Srinivas, Subramanian
Carbohydrate Research, 1996 , vol. 285, p. 159 - 165
反应条件
1: benzene; ammonia 2: Behandeln des Reaktionsprodukts mit Acetanhydrid und Pyridin View Scheme
参考文献
Hickinbottom
Journal of the Chemical Society, 1928 , p. 3140,3146
反应条件
pyridine Yield given. Yields of byproduct given;
参考文献
Koto, Shinkiti; Morishima, Naohiko; Araki, Mihoko; Tsuchiya, Takuji; Zen, Shonosuke
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 6 p. 1895 - 1896
参考文献
Montgomery et al.
Journal of the American Chemical Society, 1942 , vol. 64, p. 690,693
Journal of the American Chemical Society, 1943 , vol. 65, p. 3,6
参考文献
Hurd; Bonner
Journal of Organic Chemistry, 1946 , vol. 11, p. 50,53
参考文献
Hurd; Bonner
Journal of Organic Chemistry, 1946 , vol. 11, p. 50,53
反应条件
sodium methylate in methanol; dichloromethane
参考文献
Gridley, Jonathan J.; Hacking, Andrew J.; Osborn, Helen M. I.; Spackman, David G.
Tetrahedron, 1998 , vol. 54, # 49 p. 14925 - 14946