1-苄基-4-三氟甲基苯合成路线 (共 33 条)
反应条件
palladium diacetate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=40°C; 3 h; Inert atmosphere;
参考文献
Chang, Shu-Ting; Li, Qinghan; Chiang, Ruei-Tang; Gau, Han-Mou
Tetrahedron, 2012 , vol. 68, # 21 p. 3956 - 3962
反应条件
cis,cis,cis-tetrakis[(diphenylphosphanyl)methyl]cyclopentane; potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)) in xylene T=130°C; Suzuzki cross-coupling; 20 h;
参考文献
Chahen, Ludovic; Doucet, Henri; Santelli, Maurice
Synlett, 2003 , # 11 p. 1668 - 1672
反应条件
1,5-bis-(diphenylphosphino)-pentane; potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)) in N,N-dimethyl-formamide T=80°C; Suzuki-Miyaura reaction; 12 h;
参考文献
Kuwano, Ryoichi; Yokogi, Masashi
Organic Letters, 2005 , vol. 7, # 5 p. 945 - 947
反应条件
potassium carbonate; bis[2-(diphenylphosphino)phenyl] ether; bis(η3-allyl-μ-chloropalladium(II)) in 1,1-dimethylpropan-1-ol T=80°C; 24 h;
参考文献
Kuwano, Ryoichi; Yokogi, Masashi
Chemical Communications, 2005 , # 47 p. 5899 - 5901
反应条件
1,5-bis-(diphenylphosphino)-pentane; potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)) in N,N-dimethyl-formamide T=80°C; Suzuki-Miyaura reaction; 24 h;
参考文献
Kuwano, Ryoichi; Yokogi, Masashi
Organic Letters, 2005 , vol. 7, # 5 p. 945 - 947
反应条件
caesium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in water T=90°C; Suzuki-Miyaura cross-coupling; 18 h;
参考文献
Molander, Gary A.; Elia, Maxwell D.
Journal of Organic Chemistry, 2006 , vol. 71, # 24 p. 9198 - 9202
反应条件
iodine; hypophosphorous acid in acetic acid T=60°C; 72 h;
参考文献
Gordon, Paul E.; Fry, Albert J.
Tetrahedron Letters, 2001 , vol. 42, # 5 p. 831 - 833
反应条件
potassium tert-butylate in isopropyl alcohol T=80°C; 10 h; Inert atmosphere;
参考文献
Yang, Hengquan; Li, Guang; Ma, Zhancheng; Chao, Jianbin; Guo, Zhiqiang
Journal of Catalysis, 2010 , vol. 276, # 1 p. 123 - 133
反应条件
palladium diacetate; potassium phosphate; triphenylphosphine in toluene T=90°C; Suzuki-Miyaura coupling; 16 h;
参考文献
Organic Letters, , vol. 7, # 22 p. 4875 - 4878
反应条件
3-chloroprop-1-ene; trifluoroacetic acid; cobalt(II) dibromide; zinc in acetonitrile T=20°C; Barbier type reductive cross-coupling;
参考文献
Amatore, Muriel; Gosmini, Corinne
Chemical Communications, 2008 , # 40 p. 5019 - 5021