2′-羟基-4,4′,6′-三甲氧基查耳酮合成路线 (共 25 条)
反应条件
potassium hydroxide in methanol T=20°C; Claisen condensation; 24 h;
参考文献
Singh, Om V.; Muthukrishnan; Sunderavadivelu
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2005 , vol. 44, # 12 p. 2575 - 2581
反应条件
in methanol; ethanol; water
参考文献
Hoffmann-La Roche Inc.
Patent: US4605674 A1, 1986 ;
反应条件
aluminium trichloride T=20°C; 10 h;
参考文献
Lee, Yean-Jang; Wu, Tsao-Dong
Journal of the Chinese Chemical Society, 2001 , vol. 48, # 2 p. 201 - 206
反应条件
aluminum tri-bromide in nitrobenzene T=20°C; 24 h;
参考文献
Lee, Yean-Jang; Wu, Tsao-Dong
Journal of the Chinese Chemical Society, 2001 , vol. 48, # 2 p. 201 - 206
反应条件
potassium carbonate in acetone Heating;
参考文献
Smith, Jeffrey A.; Maloney, David J.; Hecht, Sidney M.; Lannigan, Deborah A.
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 14 p. 5018 - 5034
反应条件
potassium carbonate in acetone T=20°C; Methylation;
参考文献
Journal of Agricultural and Food Chemistry, , vol. 48, # 5 p. 1888 - 1891
反应条件
1: 98 percent / ZnCl2 2: 96 percent / 50 percent aq. KOH / ethanol / 6 h / 20 °C 3: 91 percent / AlCl3 / 10 h / 20 °C View Scheme
参考文献
Journal of the Chinese Chemical Society, , vol. 48, # 2 p. 201 - 206
反应条件
1: 96 percent / 50 percent aq. KOH / ethanol / 6 h / 20 °C 2: 91 percent / AlCl3 / 10 h / 20 °C View Scheme
参考文献
Journal of the Chinese Chemical Society, , vol. 48, # 2 p. 201 - 206
反应条件
1: 1.5 g / anhyd. potassium carbonate / acetone / 5 h / Heating 2: 400 mg / 60percent aq. NaOH / ethanol / 80 h / Ambient temperature View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 26, p. 57 - 58
反应条件
pyridine; iodine 8 h; Heating;
参考文献
Lee, Yean-Jang; Wu, Tsao-Dong
Journal of the Chinese Chemical Society, 2001 , vol. 48, # 2 p. 201 - 206