3-氯-5,6-二苯基-1,2,4-三嗪合成路线 (共 31 条)
反应条件
trichlorophosphate T=150°C;
参考文献
Johnstone, Robert A. W.; Price, Peter J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1069 - 1076
反应条件
1: 85 percent / acetic acid / 3 h / Heating 2: 66 percent / N,N-dimethylaniline, phosphorus oxychloride / 3 h / Heating View Scheme
参考文献
Johnstone, Robert A. W.; Price, Peter J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1069 - 1076
反应条件
hydrogenchloride; sodium nitrite 1) CHCl3, 0 deg C, 1.5 h, 2) r.t., 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Gonsalves, Antonio M. d'A. Rocha; Melo, Teresa M. V. D. Pinho e
Tetrahedron, 1992 , vol. 48, # 33 p. 6821 - 6826
反应条件
KNH2 in ammonia T=-33°C; 1 h; 15N labelled ammonia, other substituents in 3 position in 5,6-diphenyl-1,2,4-triazines; Mechanism;
参考文献
El-Khoshnieh, Yehia O.
Phosphorus, Sulfur and Silicon and Related Elements, 1998 , vol. 139, p. 163 - 172
反应条件
in diethyl ether; benzene 5 h; Heating; Further byproducts given;
参考文献
Zaher, H. A.; Ibrahim, Y. A.; Sherif, O.; Mohammady, R.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 6 p. 559 - 561
反应条件
in diethyl ether; benzene 5 h; Heating; MechanismProduct distribution;
参考文献
Zaher, H. A.; Ibrahim, Y. A.; Sherif, O.; Mohammady, R.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 6 p. 559 - 561
反应条件
in ethanol 48 h; Heating;
参考文献
Konno, Shoetsu; Yokoyama, Masaaki; Kaite, Akiko; Yamatsuta, Ikuko; Ogawa, Shigeru; et. al.
Chemical & Pharmaceutical Bulletin, 1982 , vol. 30, # 1 p. 152 - 157
反应条件
in diethyl ether; benzene 5 h; Heating; Further byproducts given;
参考文献
Zaher, H. A.; Ibrahim, Y. A.; Sherif, O.; Mohammady, R.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 6 p. 559 - 561
反应条件
in diethyl ether; benzene 5 h; Heating; MechanismProduct distribution;
参考文献
Zaher, H. A.; Ibrahim, Y. A.; Sherif, O.; Mohammady, R.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 6 p. 559 - 561
反应条件
in diethyl ether; benzene 5 h; Heating; Further byproducts given;
参考文献
Zaher, H. A.; Ibrahim, Y. A.; Sherif, O.; Mohammady, R.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 6 p. 559 - 561