N-丙酮基邻苯二甲酰亚胺合成路线 (共 30 条)
反应条件
in N,N-dimethyl-formamide T=20°C;
参考文献
Han, Minsoo; Nam, Kee Dal; Shin, Dongyun; Jeong, Nakcheol; Hahn, Hoh-Gyu
Journal of Combinatorial Chemistry, 2010 , vol. 12, # 4 p. 518 - 530
反应条件
jones reagent; osmium(VIII) oxide in water; acetone 20 h; Ambient temperature;
参考文献
Henry, James R.; Weinreb, Steven M.
Journal of Organic Chemistry, 1993 , vol. 58, # 17 p. 4745
反应条件
dicobalt octacarbonyl T=20°C; P=760.051 Torr; 24 h;
参考文献
Journal of Organic Chemistry, , vol. 72, # 25 p. 9630 - 9634
反应条件
bis(benzonitrile)palladium(II) dichloride; AgNO2; CuCl2·2H2O; nitromethane; oxygen; tert-butyl alcohol T=20°C; Wacker Oxidation; P=760.051 Torr; 6 h;
参考文献
Wickens, Zachary K.; Morandi, Bill; Grubbs, Robert H.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 43 p. 11257 - 11260
Angew. Chem., 2013 , vol. 125, # 43 p. 11467 - 11470
反应条件
potassium carbonate T=90 - 110°C; 3 - 4 h;
参考文献
EP1640367 A1, ;
Page/Page column 12-13 ;
反应条件
tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide in decane; ethyl acetate T=130°C; 3 h; Sealed tube;
参考文献
Lv, Yunhe; Li, Yan; Xiong, Tao; Lu, Yu; Liu, Qun; Zhang, Qian
Chemical Communications, 2014 , vol. 50, # 18 p. 2367 - 2369
反应条件
1: With hydrogen fluoride; SbF5 T=-50°C; 0.166667 h; 2: With sodium carbonate cooling; Further stages.;
参考文献
Journal of Organic Chemistry, , vol. 73, # 7 p. 2875 - 2878
反应条件
T=20°C; 0.25 h; Ionic liquid;
参考文献
Gupta, Pankaj; Rouf, Abdul; Shah, Bhahwal A.; Mukherjee, Debaraj; Taneja, Subhash C.
Synthetic Communications, 2013 , vol. 43, # 4 p. 505 - 519
反应条件
1: phthalimide With sodium hydride in tetrahydrofuran T=20 - 40°C; 1 h; 2: chloroacetone in tetrahydrofuran 15 h; Heating / reflux;
参考文献
WO2004/69806 A2, ;
Page/Page column 26-27 ;
反应条件
tert.-butylhydroperoxide; silver hexafluoroantimonate; [Pd(Quinox)Cl2] in dichloromethane; water T=20°C; 18 h; Darkness;
参考文献
Michel, Brian W.; McCombs, Jessica R.; Winkler, Andrea; Sigman, Matthew S.
Angewandte Chemie - International Edition, 2010 , vol. 49, # 40 p. 7312 - 7315