反应条件
1: 1.) 1,1,1,3,3,3,-hexamethyldisilazane, ammonium sulfate, 2.) SnCl4, TMSOTf / 1.) reflux, 2 h, 2.) 1,2-dichloroethane, RT, 2 h 2: TBAF / tetrahydrofuran / 8 h / Ambient temperature View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 40, # 2 p. 168 - 180