N-(4-溴-2-甲酰基苯基)-4-甲基苯磺酰胺合成路线 （共 10 条）
反应条件
bromine; sodium acetate in water; acetic acid T=20°C; 4 h;
参考文献
Nishiguchi, Atsuko; Ikemoto, Tomomi; Ito, Tatsuya; Miura, Shotaro; Tomimatsu, Kiminori
Heterocycles, 2007 , vol. 71, # 5 p. 1183 - 1192
反应条件
potassium carbonate in water; dimethyl sulfoxide T=130°C; 1 h;
参考文献
Nishiguchi, Atsuko; Ikemoto, Tomomi; Ito, Tatsuya; Miura, Shotaro; Tomimatsu, Kiminori
Heterocycles, 2007 , vol. 71, # 5 p. 1183 - 1192
反应条件
morpholine; sodium bis(2-methoxyethoxy)aluminium dihydride in toluene T=-10°C; 2 h;
参考文献
Nishiguchi, Atsuko; Ikemoto, Tomomi; Ito, Tatsuya; Miura, Shotaro; Tomimatsu, Kiminori
Heterocycles, 2007 , vol. 71, # 5 p. 1183 - 1192
反应条件
manganese(IV) oxide in dichloromethane T=20°C; 3 h; Inert atmosphereReflux;
参考文献
Yang, Tingting; Zhang, Tao; Yang, Shangdong; Chen, Shanshan; Li, Xingwei
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 25 p. 4290 - 4294
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=0 - 20°C; 1.5 h; Inert atmosphere;
参考文献
Kothandaraman, Prasath; Koh, Bing Qin; Limpanuparb, Taweetham; Hirao, Hajime; Chan, Philip Wai Hong
Chemistry - A European Journal, 2013 , vol. 19, # 6 p. 1978 - 1985
反应条件
1: 95 percent / pyridine / tetrahydrofuran / 1.5 h / 20 °C 2: 80 percent / MnO2 / acetone / 15 h / 20 °C 3: 93 percent / AcONa; Br2 / acetic acid; H2O / 4 h / 20 °C View Scheme
参考文献
Nishiguchi, Atsuko; Ikemoto, Tomomi; Ito, Tatsuya; Miura, Shotaro; Tomimatsu, Kiminori
Heterocycles, 2007 , vol. 71, # 5 p. 1183 - 1192
反应条件
1: triethylamine / tetrahydrofuran; water / 3 h / 20 °C / |Inert atmosphere 2: lithium aluminium tetrahydride / tetrahydrofuran / 1.5 h / 0 - 20 °C / |Inert atmosphere View Scheme
参考文献
Kuznetsov, Alexey; Makarov, Anton; Rubtsov, Aleksandr E.; Butin, Alexander V.; Gevorgyan, Vladimir
Journal of Organic Chemistry, 2013 , vol. 78, # 23 p. 12144 - 12153
反应条件
1: 95 percent / pyridine / tetrahydrofuran / 1.5 h / 20 °C 2: 80 percent / MnO2 / acetone / 15 h / 20 °C 3: 93 percent / AcONa; Br2 / acetic acid; H2O / 4 h / 20 °C View Scheme
参考文献
Nishiguchi, Atsuko; Ikemoto, Tomomi; Ito, Tatsuya; Miura, Shotaro; Tomimatsu, Kiminori
Heterocycles, 2007 , vol. 71, # 5 p. 1183 - 1192
反应条件
1: 80 percent / MnO2 / acetone / 15 h / 20 °C 2: 93 percent / AcONa; Br2 / acetic acid; H2O / 4 h / 20 °C View Scheme
参考文献
Nishiguchi, Atsuko; Ikemoto, Tomomi; Ito, Tatsuya; Miura, Shotaro; Tomimatsu, Kiminori
Heterocycles, 2007 , vol. 71, # 5 p. 1183 - 1192
反应条件
1: 87 percent / pyridine / 3 h / 20 °C 2: 50 percent / Red-Al; morpholine / toluene / 2 h / -10 °C View Scheme
参考文献
Nishiguchi, Atsuko; Ikemoto, Tomomi; Ito, Tatsuya; Miura, Shotaro; Tomimatsu, Kiminori
Heterocycles, 2007 , vol. 71, # 5 p. 1183 - 1192
